2-bromo-3-5-dinitroacetophenone

Base Information

• Chemical Name: 2-bromo-3-5-dinitroacetophenone
• CAS No.: 5000-68-0
• Molecular Formula: C₈H₅BrN₂O₅
• Molecular Weight: 289.042
• Hs Code.: 2914700090
• Mol file: 5000-68-0.mol

Synonyms:2-bromo-3-5-dinitroacetophenone

Chemical Property of 2-bromo-3-5-dinitroacetophenone

Chemical Property:

• PSA: 108.71000
• LogP: 3.12700

Purity/Quality:

95% ^*data from raw suppliers

2-BROMO-3',5'-DINITROACETOPHENONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-bromo-3-5-dinitroacetophenone

There total 1 articles about 2-bromo-3-5-dinitroacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3,5-dinitrophenyl)ethanone (14401-75-3) → 2-bromo-1-(3,5-dinitro-phenyl)-ethanone (5000-68-0)

Guidance literature:

With aluminium trichloride; bromine;

Reference yield:

2-bromo-1-(3,5-dinitro-phenyl)-ethanone (5000-68-0) → C9H9N3OS (1435388-16-1)

Guidance literature:

Multi-step reaction with 3 steps

1: acetone / 0.5 h / 20 °C / Inert atmosphere

2: sulfuric acid; acetic acid / 1 h / 100 °C / Inert atmosphere

3: iron; ammonium chloride / ethanol / 1 h / 80 °C / Inert atmosphere

With sulfuric acid; iron; ammonium chloride; acetic acid; In ethanol; acetone;

DOI:10.1021/jm301793a

Reference yield:

2-bromo-1-(3,5-dinitro-phenyl)-ethanone (5000-68-0) → C9H5N3O5S

Guidance literature:

Multi-step reaction with 2 steps

1: acetone / 0.5 h / 20 °C / Inert atmosphere

2: sulfuric acid; acetic acid / 1 h / 100 °C / Inert atmosphere

With sulfuric acid; acetic acid; In acetone;

DOI:10.1021/jm301793a

upstream raw materials:

1-(3,5-dinitrophenyl)ethanone

Downstream raw materials:

C₉H₉N₃OS