(2-Bromophenyl)methoxyazanium;chloride

Base Information

• Chemical Name: (2-Bromophenyl)methoxyazanium;chloride
• CAS No.: 51572-91-9
• Molecular Formula: C7H9BrClNO
• Molecular Weight: 238.512
• Hs Code.: 2922199090
• DSSTox Substance ID: DTXSID50370720
• Mol file: 51572-91-9.mol

Synonyms:(2-bromophenyl)methoxyazanium;chloride;SCHEMBL1715773;DTXSID50370720;AKOS005082204;O-(2-Bromobenzyl)hydroxylaminehydrochloride

Chemical Property of (2-Bromophenyl)methoxyazanium;chloride

Chemical Property:

• Melting Point: 144-146°C
• PSA: 35.25000
• LogP: 3.34170
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 236.95560
• Heavy Atom Count: 11
• Complexity: 99.6

Purity/Quality:

99% ^*data from raw suppliers

1-[(Ammoniooxy)methyl]-2-bromobenzene chloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)CO[NH3+])Br.[Cl-]

Technology Process of (2-Bromophenyl)methoxyazanium;chloride

There total 4 articles about (2-Bromophenyl)methoxyazanium;chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.19%

O-(o-bromobenzyl)acetoxime → 1-((ammoniooxy)methyl)-2-bromobenzene chloride (51572-91-9)

Guidance literature:

With hydrogenchloride; In methanol; water; at 35 ℃; for 3.33333h;

Reference yield: 62.2%

C9H10BrNO2 → 1-((ammoniooxy)methyl)-2-bromobenzene chloride (51572-91-9)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 65 ℃;

DOI:10.1016/j.bioorg.2019.103150

Reference yield:

O-(2-bromobenzyl)hydroxylamine → 1-((ammoniooxy)methyl)-2-bromobenzene chloride (51572-91-9)

Guidance literature:

With hydrogenchloride; In diethyl ether; Inert atmosphere;

DOI:10.1016/j.ejmech.2015.12.028

upstream raw materials:

1-Bromo-2-bromomethyl-benzene

Downstream raw materials:

Ph(3-Cl)(5-OCF₃)-(R)CH(OH)C(O)-Aze-Pab(OBn(2-Br))

C₂₂H₂₅BrN₂O₆S

C₂₂H₂₅BrN₂O₆S

C₁₇H₁₇BrN₂O₄S