2-(HYDROXYAMINO)-2-METHYL-1-PHENYLPROPAN-1-ONE OXIME

Base Information

• Chemical Name: 2-(HYDROXYAMINO)-2-METHYL-1-PHENYLPROPAN-1-ONE OXIME
• CAS No.: 5291-08-7
• Molecular Formula: C10H14N2O2
• Molecular Weight: 194.233
• Hs Code.: 2928000090
• Mol file: 5291-08-7.mol

Synonyms:2-(HYDROXYAMINO)-2-METHYL-1-PHENYLPROPAN-1-ONE OXIME

Chemical Property of 2-(HYDROXYAMINO)-2-METHYL-1-PHENYLPROPAN-1-ONE OXIME

Chemical Property:

• Vapor Pressure: 6.62E-06mmHg at 25°C
• Melting Point: 153-154
• Refractive Index: 1.538
• Boiling Point: 363°Cat760mmHg
• Flash Point: 173.3°C
• PSA: 64.85000
• Density: 1.12g/cm³
• LogP: 2.01320

Purity/Quality:

98% ^*data from raw suppliers

2-(HYDROXYAMINO)-2-METHYL-1-PHENYLPROPAN-1-ONE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: R34:Causes burns.
• Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S36/37/39:Wear suitabl

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(HYDROXYAMINO)-2-METHYL-1-PHENYLPROPAN-1-ONE OXIME

There total 2 articles about 2-(HYDROXYAMINO)-2-METHYL-1-PHENYLPROPAN-1-ONE OXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-2-methyl-1-phenyl-propan-1-one (10409-54-8) → N-(2-methyl-1-oximino-1-phenyl-2-propyl)hydroxylamine (5291-08-7)

Guidance literature:

With hydroxylamine hydrochloride; sodium methylate; In methanol; at 20 ℃; Heating;

DOI:10.3390/molecules25143118

Reference yield:

→ N-(2-methyl-1-oximino-1-phenyl-2-propyl)hydroxylamine (5291-08-7)

Guidance literature:

α-Brom-isobutyrophenon, Hydroxylamin-hydrochlorid, methanol. NaOH;

Reference yield: 95.0%

N-(2-methyl-1-oximino-1-phenyl-2-propyl)hydroxylamine (5291-08-7) + cyclohexane-1,2-dione (765-87-7) → 5,5-dimethyl-1-hydroxy-2-(spirocyclohexan-2-one 2)-4-phenyl-3-imidazoline 3-oxide (82811-27-6)

Guidance literature:

In methanol; for 6h; Heating;

DOI:10.1007/BF00949952

upstream raw materials:

2-bromo-2-methyl-1-phenyl-propan-1-one

Downstream raw materials:

2-Furan-2-yl-5,5-dimethyl-3-oxy-4-phenyl-2,5-dihydro-imidazol-1-ol

2-benzoyl-4-hydroxy-5,5-dimethyl-4-phenyl-2-imidazoline 3-oxide

5,5-dimethyl-1-hydroxy-2-(spirocyclohexan-2-one 2)-4-phenyl-3-imidazoline 3-oxide

2-acetyl-4-hydroxy-5,5-dimethyl-4-phenyl-2-imidazoline 3-oxide

Refernces