N-(3,4,6-TRI-O-ACETYL-BETA-D-GLUCOPYRANOSYL) PIPERIDINE

Base Information

• Chemical Name: N-(3,4,6-TRI-O-ACETYL-BETA-D-GLUCOPYRANOSYL) PIPERIDINE
• CAS No.: 52389-39-6
• Molecular Formula: C₁₇H₂₇NO₈
• Molecular Weight: 373.403
• Hs Code.: 29333990
• Mol file: 52389-39-6.mol

Synonyms:N-(3,4,6-TRI-O-ACETYL-BETA-D-GLUCOPYRANOSYL) PIPERIDINE;N-TRI-O-ACETYL-BETA-D-GLUCOPYRANOSYL PIPERIDINE;2,3,4-TRI-O-ACETYL-BETA-D-ARABINOPYRANOSYL CYANIDE;N-(3,4,6-Tri-O-acetyl-b-D-glucopyranosyl)piperidine;N-(3,4,6-TRI-O-ACETYL-SS-D-GLUCOPYRANOSYL) PIPERIDINE

Chemical Property of N-(3,4,6-TRI-O-ACETYL-BETA-D-GLUCOPYRANOSYL) PIPERIDINE

Chemical Property:

• Melting Point: 136 - 137 °C
• PSA: 111.60000
• LogP: -0.07750

Purity/Quality:

99%, ^*data from raw suppliers

N-(3-4-6-Tri-O-acetyl-β-D-glucopyranosyl)piperidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(3,4,6-TRI-O-ACETYL-BETA-D-GLUCOPYRANOSYL) PIPERIDINE

There total 6 articles about N-(3,4,6-TRI-O-ACETYL-BETA-D-GLUCOPYRANOSYL) PIPERIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

piperidine (110-89-4) + β-D-glucose pentaacetate (604-69-3) → N-<3,4,6-tri-O-acetyl-β-D-glucopyranosyl>piperidine (36215-42-6,52389-39-6)

Guidance literature:

at 20 - 25 ℃; for 0.75h;

DOI:10.1002/jlcr.2933

Reference yield: 33.2%

piperidine (110-89-4) + β-D-glucose pentaacetate (604-69-3) → N-<3,4,6-tri-O-acetyl-β-D-glucopyranosyl>piperidine (36215-42-6,52389-39-6) + N-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)piperidine (91290-05-0) + N-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)piperidine

Guidance literature:

In diethyl ether; for 0.333333h; Ambient temperature;

DOI:10.1016/S0008-6215(99)00029-4

Reference yield: 25.0%

piperidine (110-89-4) + α-D-glucopyranose peracetylate (604-68-2) → N-<3,4,6-tri-O-acetyl-β-D-glucopyranosyl>piperidine (36215-42-6,52389-39-6)

Guidance literature:

In diethyl ether;

DOI:10.1016/S0040-4039(99)00928-4

upstream raw materials:

piperidine

2,3,4,6-tetra-O-acetyl-β-D-glucopyranose

β-D-glucose pentaacetate

α-D-glucopyranose peracetylate

Downstream raw materials:

(1R)-O³,O⁴,O⁶-triacetyl-O²-phenylcarbamoyl-1-piperidino-1,5-anhydro-D-glucitol

3,4,6-tri-O-acetyl-2-O-benzyl-1-deoxy-1-piperidino-β-D-glucopyranose

N-(2,O-allyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-piperidine

1-O-acetyl-2-O-allyl-3,4,6-tri-O-benzyl-α-D-glucose

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