Hexyl Glyoxylate

Base Information

• Chemical Name: Hexyl Glyoxylate
• CAS No.: 52709-43-0
• Molecular Formula: C8H14O3
• Molecular Weight: 158.197
• Hs Code.: 2918300090
• Mol file: 52709-43-0.mol

Synonyms:Glyoxylsaeure-n-hexylester;Hexyl Glyoxylate;Oxo-acetic Acid Hexyl Este;Oxo-acetic Acid Hexyl Ester

Chemical Property of Hexyl Glyoxylate

Chemical Property:

• Vapor Pressure: 0.161mmHg at 25°C
• Refractive Index: 1.423
• Boiling Point: 213.8°C at 760 mmHg
• Flash Point: 82.623°C
• PSA: 43.37000
• Density: 0.98g/cm³
• LogP: 1.30880

Purity/Quality:

99% ^*data from raw suppliers

HexylGlyoxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Hexyl Glyoxylate is a glyoxylic ester, useful precursor in the synthesis of novel low molecular weight metalloporphyrins.

Technology Process of Hexyl Glyoxylate

There total 4 articles about Hexyl Glyoxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-n-hexyl tartrate (155602-83-8) → n-hexyl glyoxylate (52709-43-0)

Guidance literature:

With periodic acid; In diethyl ether; at 0 ℃; for 2.5h;

DOI:10.1016/S0968-0896(03)00272-4

Reference yield:

hexan-1-ol (111-27-3) → n-hexyl glyoxylate (52709-43-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 25 percent / H₂SO₄ / Heating

2: periodic acid dihydrate / diethyl ether / 2.5 h / 0 °C

With sulfuric acid; periodic acid; In diethyl ether;

DOI:10.1016/S0968-0896(03)00272-4

Reference yield:

→ glyoxylic ester + n-hexyl glyoxylate (52709-43-0)

Guidance literature:

upstream raw materials:

di-n-hexyl tartrate

hexan-1-ol