Furan-3,4-dicarbonyl dichloride

Base Information

Chemical Name:Furan-3,4-dicarbonyl dichloride
CAS No.:52762-41-1
Molecular Formula:C6H2Cl2O3
Molecular Weight:192.98
Hs Code.:2932190090
DSSTox Substance ID:DTXSID20503260
Mol file:52762-41-1.mol

Synonyms:52762-41-1;furan-3,4-dicarbonyl dichloride;3,4-furandicarbonyl chloride;SCHEMBL7231260;DTXSID20503260

Suppliers and Price of Furan-3,4-dicarbonyl dichloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Furan-3,4-dicarbonyl dichloride

Chemical Property:

PSA：47.28000
LogP:2.03760
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:191.9380993
Heavy Atom Count:11
Complexity:172

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C(=CO1)C(=O)Cl)C(=O)Cl

Technology Process of Furan-3,4-dicarbonyl dichloride

There total 4 articles about Furan-3,4-dicarbonyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3387-26-6
furan-3,4-dicarboxylic acid

: 52762-41-1
furan-3,4-dicarbonyl dichloride

Guidance literature:: With thionyl chloride; In toluene; for 3h; Heating;
DOI:10.1002/jhet.5570300624

Reference yield:

: 4282-33-1
dimethyl 3,4-furandicarboxylate

: 52762-41-1
furan-3,4-dicarbonyl dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / Reflux

2: oxalyl dichloride / Reflux

With oxalyl dichloride; potassium hydroxide; In ethanol;

Reference yield:

: 30614-77-8
diethyl 3,4-furandicarboxylate

: 52762-41-1
furan-3,4-dicarbonyl dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: 3N aq. NaOH / methanol / a) RT, 1.5 h, b) reflux, 0.75 h

2: 98 percent / thionyl chloride / toluene / 3 h / Heating

With sodium hydroxide; thionyl chloride; In methanol; toluene;
DOI:10.1002/jhet.5570300624