2-[(Dimethylamino)methylidene]decanal

Base Information

Chemical Name:2-[(Dimethylamino)methylidene]decanal
CAS No.:57202-67-2
Molecular Formula:C₁₃H₂₅NO
Molecular Weight:211.348
Hs Code.:
DSSTox Substance ID:DTXSID20708233
Mol file:57202-67-2.mol

Synonyms:57202-67-2;2-[(DIMETHYLAMINO)METHYLIDENE]DECANAL;SCHEMBL6971674;DTXSID20708233

Suppliers and Price of 2-[(Dimethylamino)methylidene]decanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-[(Dimethylamino)methylidene]decanal

Chemical Property:

PSA：20.31000
LogP:3.38140
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:211.193614421
Heavy Atom Count:15
Complexity:185

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCC(=CN(C)C)C=O

Technology Process of 2-[(Dimethylamino)methylidene]decanal

There total 2 articles about 2-[(Dimethylamino)methylidene]decanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34764-02-8
decanal diethyl acetal

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 3-ethoxy-2-n-octyl-prop-2-enal

: 57202-67-2
2-(N,N-dimethylaminomethylidene)decanal

Guidance literature:: With trichlorophosphate; In neat (no solvent); at 70 - 75 ℃; for 2h; Schlenk technique;
DOI:10.1039/c6dt00847j

Reference yield:

: 112-31-2
caprinaldehyde

: 3-ethoxy-2-n-octyl-prop-2-enal

: 57202-67-2
2-(N,N-dimethylaminomethylidene)decanal

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / ethanol / 1 h / 20 °C

2: trichlorophosphate / neat (no solvent) / 2 h / 70 - 75 °C / Schlenk technique

With toluene-4-sulfonic acid; trichlorophosphate; In ethanol;
DOI:10.1039/c6dt00847j