N-OCTYLTRIBUTYLPHOSPHONIUM BROMIDE

Base Information

• Chemical Name: N-OCTYLTRIBUTYLPHOSPHONIUM BROMIDE
• CAS No.: 57702-65-5
• Molecular Formula: C20H44BrP
• Molecular Weight: 395.44
• Mol file: 57702-65-5.mol

Synonyms:N-OCTYLTRIBUTYLPHOSPHONIUM BROMIDE;TRIBUTYL-N-OCTYLPHOSPHONIUM BROMIDE;TRIBUTYL(OCTYL)PHOSPHONIUM BROMIDE;HISHICOLIN PX-48B;n-Octyltri-n-butylphosphonium Bromide

Chemical Property of N-OCTYLTRIBUTYLPHOSPHONIUM BROMIDE

Chemical Property:

• Melting Point: 25 °C
• PSA: 13.59000
• LogP: 4.76880

Purity/Quality:

98%,99%, ^*data from raw suppliers

Tributyl(octyl)phosphoniumBromide ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-OCTYLTRIBUTYLPHOSPHONIUM BROMIDE

There total 1 articles about N-OCTYLTRIBUTYLPHOSPHONIUM BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-octane (111-83-1) + tributylphosphine (998-40-3) → octyltributylphosphonium bromide (57702-65-5)

Guidance literature:

at 80 ℃; Inert atmosphere;

DOI:10.1016/j.electacta.2010.08.106

Reference yield:

octyltributylphosphonium bromide (57702-65-5) → C20H44P(1+)*C8H11O2(1-)

Guidance literature:

Multi-step reaction with 2 steps

1: DowexMonosphere 550A (OH)

2: ethanol / 12 h / 20 °C

With DowexMonosphere 550A (OH); In ethanol;

DOI:10.1002/anie.201701919

upstream raw materials:

1-bromo-octane

tributylphosphine

Refernces

• 1、 -. "Mercaptopyrimidine anti-corrosive ionic liquid as well as preparation method and application thereof". Paragraph 0029; 0032; 0035. . Retrieved 2019/01/07.
• 2、 Rauber, Daniel,Zhang, Peng,Huch, Volker,Kraus, Tobias,Hempelmann, Rolf. "Lamellar structures in fluorinated phosphonium ionic liquids: The roles of fluorination and chain length". . p. 27251 - 27258. Retrieved 2017/10/27.