N-(3-AMINOPROPYL)-N-METHYLANILINE

Base Information

• Chemical Name: N-(3-AMINOPROPYL)-N-METHYLANILINE
• CAS No.: 53485-07-7
• Molecular Formula: C10H16N2
• Molecular Weight: 164.25
• Hs Code.: 2921599090
• Mol file: 53485-07-7.mol

Synonyms:AKOS BC-2002;N-(3-AMINOPROPYL)-N-METHYLANILINE;N*1*-METHYL-N*1*-PHENYL-PROPANE-1,3-DIAMINE;N1-METHYL-N1-PHENYL-PROPANE-1,3-DIAMINE;RARECHEM AL BW 0401;Aminopropylmethylaniline;n-(3-aminopropyl)-n-methylaniline96+%

Chemical Property of N-(3-AMINOPROPYL)-N-METHYLANILINE

Chemical Property:

• Refractive Index: 1.563
• Boiling Point: 266.7°Cat760mmHg
• Flash Point: 104.2°C
• PSA: 29.26000
• Density: 1g/cm³
• LogP: 2.17190
• Storage Temp.: Refrigerator, Under inert atmosphere
• Solubility.: Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-(3-Aminopropyl)-N-methylaniline ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(3-AMINOPROPYL)-N-METHYLANILINE

There total 4 articles about N-(3-AMINOPROPYL)-N-METHYLANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-cyanoethyl)-N-methylaniline (94-34-8) → N-(3-aminopropyl)-N-methylaniline (53485-07-7)

Guidance literature:

With ammonia; nickel; at 103 ℃; under 50014.5 Torr; Hydrogenation;

DOI:10.1021/ja01233a019

Reference yield:

N-methylaniline (100-61-8) → N-(3-aminopropyl)-N-methylaniline (53485-07-7)

Guidance literature:

Multi-step reaction with 2 steps

1: copper (II)-sulfate / 180 °C

2: Raney nickel; ethanolic ammonia / 103 °C / 50014.5 Torr / Hydrogenation

With ammonia; nickel; copper(II) sulfate;

DOI:10.1021/ja01233a019

Reference yield:

N-(3-chloro-propyl)-N-methyl-aniline (128622-94-6) → N-(3-aminopropyl)-N-methylaniline (53485-07-7) + bis-[3-(N-methyl-anilino)-propyl]-amine (854253-71-7)

Guidance literature:

With ammonia;

upstream raw materials:

N-(2-cyanoethyl)-N-methylaniline

N-(3-chloro-propyl)-N-methyl-aniline

N-methylaniline

Downstream raw materials:

N-[3-(N-methyl-anilino)-propyl]-acetamide

C₁₄H₁₆N₂O₂

C₃₁H₃₈N₈O₈

Fast Corinth V salt

Refernces