N-BENZYL-2-NITROANILINE

Base Information

• Chemical Name: N-BENZYL-2-NITROANILINE
• CAS No.: 5729-06-6
• Molecular Formula: C13H12N2O2
• Molecular Weight: 228.25
• Hs Code.: 2921420090
• Mol file: 5729-06-6.mol

Synonyms:N-BENZYL-2-NITROANILINE;BENZYL-2-NITROANILINE;N-Benezyl-2-nitroaniline

Chemical Property of N-BENZYL-2-NITROANILINE

Chemical Property:

• Vapor Pressure: 4.75E-06mmHg at 25°C
• Refractive Index: 1.658
• Boiling Point: 382.3°C at 760 mmHg
• Flash Point: 185°C
• PSA: 57.85000
• Density: 1.258g/cm³
• LogP: 3.80310
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

N-Benzyl-2-nitroaniline ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-BENZYL-2-NITROANILINE

There total 27 articles about N-BENZYL-2-NITROANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

o-nitroiodobenzene (609-73-4) + benzylamine (100-46-9) → N-benzyl-2-nitroaniline (5729-06-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 2h; Inert atmosphere;

DOI:10.1002/ejoc.201000149

Reference yield: 98.0%

ortho-nitrofluorobenzene (1493-27-2,127723-77-7) + benzylamine (100-46-9) → N-benzyl-2-nitroaniline (5729-06-6)

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃;

Reference yield: 97.0%

2-Chloronitrobenzene (88-73-3) + benzylamine (100-46-9) → N-benzyl-2-nitroaniline (5729-06-6)

Guidance literature:

With ammonium acetate; at 100 ℃; for 24h;

DOI:10.1021/jm00164a051

upstream raw materials:

benzyl chloride

2-nitro-aniline

2-Chloronitrobenzene

benzylamine

Downstream raw materials:

N-benzyl-1,2-phenylenediamine

[benzyl-(2-nitro-phenyl)-sulfamoyl]-acetic acid ethyl ester

Benzyl-(2-nitro-phenyl)-carbamic acid ethyl ester

1-benzylbenzimidazole