3-ACETYLNORADAMANTANE TECH. 85

Base Information

• Chemical Name: 3-ACETYLNORADAMANTANE TECH. 85
• CAS No.: 58275-58-4
• Molecular Formula: C11H16O
• Molecular Weight: 164.24414
• Mol file: 58275-58-4.mol

Synonyms:1-(Octahydro-2,5-methanopentalen-1-yl)ethanone;1-(Tricyclo[3.3.1.0~3,7~]non-2-yl)ethanone;ethanone, 1-(octahydro-2,5-methanopentalen-1-yl)-;

Chemical Property of 3-ACETYLNORADAMANTANE TECH. 85

Chemical Property:

• Vapor Pressure: 0.0207mmHg at 25°C
• Refractive Index: 1.524
• Boiling Point: 251.2°Cat760mmHg
• Flash Point: 97.2°C
• Density: 1.073g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 3-ACETYLNORADAMANTANE TECH. 85

There total 4 articles about 3-ACETYLNORADAMANTANE TECH. 85 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

endo-Bicyclo<3.2.1>oct-6-en-3-ylessigsaeure (29603-52-9) → 2-endo-Acetylnoradamantan (58275-58-4)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) aq. NaOH, (ii) oxalyl dichloride, Py

2: Et₃N

3: KOtBu, DMSO

With potassium tert-butylate; dimethyl sulfoxide; triethylamine;

DOI:10.1021/jo00444a016

Reference yield:

(1R,3R,5S)-Bicyclo[3.2.1]oct-6-en-3-yl-acetyl chloride (63609-74-5) → 2-endo-Acetylnoradamantan (58275-58-4)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N

2: KOtBu, DMSO

With potassium tert-butylate; dimethyl sulfoxide; triethylamine;

DOI:10.1021/jo00444a016

Reference yield:

C10H12O → 2-endo-Acetylnoradamantan (58275-58-4)

Guidance literature:

Multi-step reaction with 2 steps

1: KOtBu, DMSO

With potassium tert-butylate; dimethyl sulfoxide;

DOI:10.1021/jo00444a016

upstream raw materials:

methyllithium

endo-Bicyclo<3.2.1>oct-6-en-3-ylessigsaeure

(1R,3R,5S)-Bicyclo[3.2.1]oct-6-en-3-yl-acetyl chloride