Carbamic acid, [(1S)-1-ethyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, [(1S)-1-ethyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)
CAS No.:628715-93-5
Molecular Formula:C₁₀H₁₉NO₂
Molecular Weight:185.266
Hs Code.:
Mol file:628715-93-5.mol

Synonyms:Carbamic acid, [(1S)-1-ethyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Carbamic acid, [(1S)-1-ethyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Carbamic acid, [(1S)-1-ethyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

PSA：38.33000
LogP:2.86660

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, [(1S)-1-ethyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI)

There total 1 articles about Carbamic acid, [(1S)-1-ethyl-2-propenyl]-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70218-47-2
C₅H₁₁N

: 24424-99-5
di-tert-butyl dicarbonate

: 628715-93-5
C₁₀H₁₉NO₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine;
DOI:10.1016/j.bmcl.2007.04.072

Reference yield:

: 628715-93-5
C₁₀H₁₉NO₂

: C₄₁H₆₅N₃O₉S

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran

2: aq. NaOH / Pd(PPh₃)4 / toluene / 85 °C

3: LiBH₄ / tetrahydrofuran

4: AgOTf; 2,6-di-t-butyl-pyridine resin / 1,2-dichloro-ethane

With sodium hydroxide; lithium borohydride; silver trifluoromethanesulfonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,2-dichloro-ethane; toluene;
DOI:10.1016/j.bmcl.2007.04.072

Reference yield:

: 628715-93-5
C₁₀H₁₉NO₂

: C₂₇H₄₁N₃O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran

2: aq. NaOH / Pd(PPh₃)4 / toluene / 85 °C

3: LiBH₄ / tetrahydrofuran

4: AgOTf; 2,6-di-t-butyl-pyridine resin / 1,2-dichloro-ethane

5: HCl / CH₂Cl₂

With hydrogenchloride; sodium hydroxide; lithium borohydride; silver trifluoromethanesulfonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; toluene;
DOI:10.1016/j.bmcl.2007.04.072