N-(2-BIPHENYL)ANTHRANILIC ACID

Base Information

Chemical Name:N-(2-BIPHENYL)ANTHRANILIC ACID
CAS No.:59304-39-1
Molecular Formula:C19H15NO2
Molecular Weight:289.334
Hs Code.:
Mol file:59304-39-1.mol

Synonyms:N-(2-BIPHENYL)ANTHRANILIC ACID

Suppliers and Price of N-(2-BIPHENYL)ANTHRANILIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-(2-BIPHENYL)ANTHRANILIC ACID 95.00%
5MG
$ 500.29

Total 3 raw suppliers

Chemical Property of N-(2-BIPHENYL)ANTHRANILIC ACID

Chemical Property:

Vapor Pressure:8.54E-10mmHg at 25°C
Melting Point:148 °C
Refractive Index:1.67
Boiling Point:474.1°C at 760 mmHg
PKA:3.68±0.36(Predicted)
Flash Point:240.5°C
PSA：49.33000
Density:1.24g/cm³
LogP:4.86840

Purity/Quality:

97% ^*data from raw suppliers

N-(2-BIPHENYL)ANTHRANILIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(2-BIPHENYL)ANTHRANILIC ACID

There total 7 articles about N-(2-BIPHENYL)ANTHRANILIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 74531-51-4
methyl 2-([1,1'-biphenyl]-2-ylamino)benzoate

: 59304-39-1
2-([1,1’-biphenyl]-2-ylamino)benzoic acid

Guidance literature:: methyl 2-([1,1'-biphenyl]-2-ylamino)benzoate; With sodium hydroxide; In methanol; water; at 70 ℃; for 1h; Inert atmosphere;

With hydrogenchloride; In methanol; water;
DOI:10.1021/acs.jmedchem.9b02107

Reference yield: 85.0%

: 90-41-5
2-phenylaniline

: 118-91-2
ortho-chlorobenzoic acid

: 59304-39-1
2-([1,1’-biphenyl]-2-ylamino)benzoic acid

Guidance literature:: With copper(I) oxide; copper; potassium carbonate; In 2-ethoxy-ethanol; at 130 ℃; for 24h;
DOI:10.1021/jo0518809

Reference yield:

: 86-00-0
2-nitrobiphenyl

: 59304-39-1
2-([1,1’-biphenyl]-2-ylamino)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium chloride; acetic acid; iron / water; methanol / 0.42 h / 50 °C

1.2: pH 9

2.1: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate / toluene / 6 h / 90 °C / Inert atmosphere

3.1: sodium hydroxide / water; methanol / 1 h / 70 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; iron; ammonium chloride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; acetic acid; sodium hydroxide; In methanol; water; toluene; 2.1: |Buchwald-Hartwig Coupling;
DOI:10.1021/acs.jmedchem.9b02107