Pentanoic acid, 2-hydrazino-4-methyl-, methyl ester, (2S)- (9CI)

Base Information

• Chemical Name: Pentanoic acid, 2-hydrazino-4-methyl-, methyl ester, (2S)- (9CI)
• CAS No.: 528852-00-8
• Molecular Formula: C₇H₁₆N₂O₂
• Molecular Weight: 160.216
• Mol file: 528852-00-8.mol

Synonyms:Pentanoic acid, 2-hydrazino-4-methyl-, methyl ester, (2S)- (9CI)

Chemical Property of Pentanoic acid, 2-hydrazino-4-methyl-, methyl ester, (2S)- (9CI)

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pentanoic acid, 2-hydrazino-4-methyl-, methyl ester, (2S)- (9CI)

There total 6 articles about Pentanoic acid, 2-hydrazino-4-methyl-, methyl ester, (2S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C17H32N2O6 → 2-hydrazino-4-methyl-valeric acid methyl ester (528852-00-8)

Guidance literature:

With trifluoroacetic acid;

DOI:10.1016/S0040-4039(99)00584-5

Reference yield:

carbonic acid ethyl ester 1-isobutyl-3-trimethylsilanyl-prop-2-ynyl ester → 2-hydrazino-4-methyl-valeric acid methyl ester (528852-00-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) Ti(O-i-Pr)4, i-PrMgCl / 1.) ether, -50 to -40 deg C, 2 h; 2.) -78 to 0 deg C, 1 h

2: 78 percent / RuCl₃, NaIO₄

3: 76 percent / NaHCO₃

4: TFA

With titanium(IV) isopropylate; ruthenium trichloride; sodium periodate; isopropylmagnesium chloride; sodium hydrogencarbonate; trifluoroacetic acid;

DOI:10.1016/S0040-4039(99)00584-5

Reference yield:

phosphoric acid diethyl ester 1-isobutyl-3-trimethylsilanyl-prop-2-ynyl ester → 2-hydrazino-4-methyl-valeric acid methyl ester (528852-00-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) Ti(O-i-Pr)4, i-PrMgCl / 1.) ether, -50 to -40 deg C, 2 h; 2.) -78 to 0 deg C, 1 h

2: 78 percent / RuCl₃, NaIO₄

3: 76 percent / NaHCO₃

4: TFA

With titanium(IV) isopropylate; ruthenium trichloride; sodium periodate; isopropylmagnesium chloride; sodium hydrogencarbonate; trifluoroacetic acid;

DOI:10.1016/S0040-4039(99)00584-5

upstream raw materials:

C₂₀H₃₈N₂O₄Si

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