2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER

Base Information

Chemical Name:2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER
CAS No.:534602-91-0
Molecular Formula:C26H37NO5Si
Molecular Weight:471.66118
Hs Code.:
Mol file:534602-91-0.mol

Synonyms:2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER

Suppliers and Price of 2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER 95.00%
5MG
$ 501.79

Total 2 raw suppliers

Chemical Property of 2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER

Chemical Property:

PSA：73.86000
LogP:4.41030

Purity/Quality:

97% ^*data from raw suppliers

2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER

There total 5 articles about 2-TERT-BUTOXYCARBONYLAMINO-4-(TERT-BUTYL-DIPHENYL-SILANYLOXY)-BUTYRIC ACID METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 534602-90-9
C₃₁H₄₅NO₇Si

: 534602-91-0
2-tert-butoxycarbonylamino-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/S0960-894X(02)01026-0

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 534602-91-0
2-tert-butoxycarbonylamino-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Et₃N / 8 h / 20 °C

2: 98 percent / dil. TFA / CH₂Cl₂ / 1 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0960-894X(02)01026-0

Reference yield:

: 224192-24-9
methyl (2S)-2-{(tert-butoxy)-N-[(tert-butyl)oxycarbonyl]carbonylamino}-4-hydroxybutanoate

: 534602-91-0
2-tert-butoxycarbonylamino-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Et₃N / 8 h / 20 °C

2: 98 percent / dil. TFA / CH₂Cl₂ / 1 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0960-894X(02)01026-0