1,8-Diazido-3,5-dioxaoctane

Base Information

• Chemical Name: 1,8-Diazido-3,5-dioxaoctane
• CAS No.: 59559-06-7
• Molecular Formula: C6H12N6O2
• Molecular Weight: 200.2
• Mol file: 59559-06-7.mol

Synonyms:1,2-Bis(2-azidoethoxy)ethane;1,8-Diazido-3,5-dioxaoctane;1-Azido-2-[2-(2-azidoethoxy)ethoxy]ethane

Chemical Property of 1,8-Diazido-3,5-dioxaoctane

Chemical Property:

• Refractive Index: n20/D 1.47
• Boiling Point: 8 °C(Press: 0.3 Torr)
• PSA: 117.96000
• Density: 1.15 g/mL
• LogP: 0.89332
• Storage Temp.: -20°C Freezer
• Solubility.: Chloroform, Methanol

Purity/Quality:

97% ^*data from raw suppliers

1,8-Diazido-3,6-dioxaoctane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,8-Diazido-3,5-dioxaoctane

There total 10 articles about 1,8-Diazido-3,5-dioxaoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 1,8-diazido-3,6-dioxaoctane (59559-06-7,82055-94-5)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2009.01.028

Reference yield: 99.0%

1,2-bis(2-chloroethoxy)ethane (112-26-5,27252-69-3) → 1,8-diazido-3,6-dioxaoctane (59559-06-7,82055-94-5)

Guidance literature:

With sodium azide; sodium iodide; In acetonitrile; for 48h; Heating;

DOI:10.1016/j.bmcl.2007.01.010

Reference yield: 96.0%

→ 1,8-diazido-3,6-dioxaoctane (59559-06-7,82055-94-5)

Guidance literature:

upstream raw materials:

1,2-bis(2-chloroethoxy)ethane

triethylene glycol di-(p-toluenesulfonate)

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

1,2-bis(2-tosylethoxy)ethane

Downstream raw materials:

3,6-dioxa-1,8-diaminooctane

C₂₈H₃₆N₆O₈

Kryptofix 21

1-{2-[2-(2-aminoethoxy)ethoxy]ethyl}-2,5-dihydro-1H-pyrrole-2,5-dione trifluoroacetate

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