5,6,7,8-TETRAHYDRO-[1,2,4]TRIAZOLO[4,3-A]PYRAZINE OXALATE

Base Information

• Chemical Name: 5,6,7,8-TETRAHYDRO-[1,2,4]TRIAZOLO[4,3-A]PYRAZINE OXALATE
• CAS No.: 59624-08-7
• Molecular Formula: C₆H₉N₃
• Molecular Weight: 123.158
• Hs Code.: 2933990090
• Mol file: 59624-08-7.mol

Synonyms:5,6,7,8-TETRAHYDRO-[1,2,4]TRIAZOLO[4,3-A]PYRAZINE OXALATE

Chemical Property of 5,6,7,8-TETRAHYDRO-[1,2,4]TRIAZOLO[4,3-A]PYRAZINE OXALATE

Chemical Property:

• PSA: 117.34000
• LogP: -1.13430

Purity/Quality:

98%min ^*data from raw suppliers

5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T
• Statements: 25
• Safety Statements: 45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,6,7,8-TETRAHYDRO-[1,2,4]TRIAZOLO[4,3-A]PYRAZINE OXALATE

There total 1 articles about 5,6,7,8-TETRAHYDRO-[1,2,4]TRIAZOLO[4,3-A]PYRAZINE OXALATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyridine (59624-08-7)

Guidance literature:

entspr. Triazolopyridin, H2;

Reference yield: 15.0%

chloro-diphenylphosphine (1079-66-9,74391-44-9) + 5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyridine (59624-08-7) → 3-(diphenylphosphoroselenoyl)-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyridine

Guidance literature:

chloro-diphenylphosphine; 5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyridine; With triethylamine; In dichloromethane; at 20 ℃;

With selenium; In benzene; at 20 ℃;

DOI:10.1002/hc.21258

Reference yield:

chloro-diphenylphosphine (1079-66-9,74391-44-9) + 5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyridine (59624-08-7) → 3-(diphenylphosphanyl)-5,6,7,8-tetrahydro-[1,2,4]triazolo[4,3-a]pyridine

Guidance literature:

Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 20 °C

1.2: 20 °C

2.1: Hexamethylphosphorous triamide / dichloromethane

With triethylamine; Hexamethylphosphorous triamide; In dichloromethane;

DOI:10.1002/hc.21258