2-Propanamine,N-[2-methyl-1-(1-methylethyl)-3-azetidinylidene]-,[N(E)]-(9CI)

Base Information

Chemical Name:2-Propanamine,N-[2-methyl-1-(1-methylethyl)-3-azetidinylidene]-,[N(E)]-(9CI)
CAS No.:547753-52-6
Molecular Formula:C10H20N2
Molecular Weight:168.28
Hs Code.:
Mol file:547753-52-6.mol

Synonyms:2-Propanamine,N-[2-methyl-1-(1-methylethyl)-3-azetidinylidene]-,[N(E)]-(9CI)

Suppliers and Price of 2-Propanamine,N-[2-methyl-1-(1-methylethyl)-3-azetidinylidene]-,[N(E)]-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-Propanamine,N-[2-methyl-1-(1-methylethyl)-3-azetidinylidene]-,[N(E)]-(9CI)

Chemical Property:

PSA：15.60000
LogP:1.88620

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2-Propanamine,N-[2-methyl-1-(1-methylethyl)-3-azetidinylidene]-,[N(E)]-(9CI)

There total 3 articles about 2-Propanamine,N-[2-methyl-1-(1-methylethyl)-3-azetidinylidene]-,[N(E)]-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 75-31-0
isopropylamine

: 547753-49-1
1-isopropyl-2-methylazetidin-3-one

: 547753-52-6
(E)-1-isopropyl-3-[(N-isopropyl)imino]-2-methylazetidine

Guidance literature:: With titanium tetrachloride; In diethyl ether; at 20 ℃; for 3h;
DOI:10.1016/S0040-4020(03)00241-2

Reference yield:

: 547753-51-5
3,3-dimethoxy-1-isopropyl-2-methylazetidine

: 547753-52-6
(E)-1-isopropyl-3-[(N-isopropyl)imino]-2-methylazetidine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 6N HCl / 12 h / Heating

2: 70 percent / TiCl₄ / diethyl ether / 3 h / 20 °C

With hydrogenchloride; titanium tetrachloride; In diethyl ether;
DOI:10.1016/S0040-4020(03)00241-2

Reference yield:

: N-(4-bromo-3,3-dimethoxy-2-butylidene)isopropylamine

: 547753-52-6
(E)-1-isopropyl-3-[(N-isopropyl)imino]-2-methylazetidine

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / NaBH₄ / methanol / 2 h / Heating

2: 91 percent / 6N HCl / 12 h / Heating

3: 70 percent / TiCl₄ / diethyl ether / 3 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; titanium tetrachloride; In methanol; diethyl ether;
DOI:10.1016/S0040-4020(03)00241-2