Cyclopropanecarbonyl chloride, 1-(3-chlorophenyl)- (9CI)

Base Information

• Chemical Name: Cyclopropanecarbonyl chloride, 1-(3-chlorophenyl)- (9CI)
• CAS No.: 501698-47-1
• Molecular Formula: C10H8Cl2O
• Molecular Weight: 215.079
• Mol file: 501698-47-1.mol

Synonyms:Cyclopropanecarbonyl chloride, 1-(3-chlorophenyl)- (9CI)

Chemical Property of Cyclopropanecarbonyl chloride, 1-(3-chlorophenyl)- (9CI)

Chemical Property:

• PSA: 17.07000
• LogP: 3.13700

Purity/Quality:

98% ^*data from raw suppliers

1-(3-Chlorophenyl)cyclopropanecarbonylchloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclopropanecarbonyl chloride, 1-(3-chlorophenyl)- (9CI)

There total 1 articles about Cyclopropanecarbonyl chloride, 1-(3-chlorophenyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-chlorophenyl)cyclopropane-1-carboxylic acid (124276-34-2) → 1-(3-chlorophenyl)cyclopropanecarbonyl chloride (501698-47-1)

Guidance literature:

With thionyl chloride; In toluene; at 115 ℃;

DOI:10.1021/jm9013696

Reference yield: 90.0%

1-(3-chlorophenyl)cyclopropanecarbonyl chloride (501698-47-1) + 4-bromo-3-(1H-tetrazol-5-yl)aniline → 4N-[4-bromo-3-(1H-tetrazol-5-yl)phenyl]-1-(3-chlorophenyl)cyclopropanecarboxamide

Guidance literature:

With pyridine; at 0 - 20 ℃; for 3h;

Reference yield: 57.0%

1-(3-chlorophenyl)cyclopropanecarbonyl chloride (501698-47-1) + 4-(6-ethoxypyridin-3-yl)-3-(1H-tetrazol-5-yl)aniline → 1-(3-chlorophenyl)-N-[4-(6-ethoxypyridin-3-yl)-3-(1H-tetrazol-5-yl)phenyl]cyclopropanecarboxamide

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 1h;

upstream raw materials:

1-(3-chlorophenyl)cyclopropane-1-carboxylic acid

Downstream raw materials:

GS⁽¹¹⁶⁾K₂₆₂₂A

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