Cyclopentanol, 4-ethylidene-2,2-dimethyl-5-methylene- (9CI)

Base Information

• Chemical Name: Cyclopentanol, 4-ethylidene-2,2-dimethyl-5-methylene- (9CI)
• CAS No.: 502497-12-3
• Molecular Formula: C10H16O
• Molecular Weight: 152.23344
• Mol file: 502497-12-3.mol

Synonyms:Cyclopentanol, 4-ethylidene-2,2-dimethyl-5-methylene- (9CI)

Chemical Property of Cyclopentanol, 4-ethylidene-2,2-dimethyl-5-methylene- (9CI)

Chemical Property:

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Technology Process of Cyclopentanol, 4-ethylidene-2,2-dimethyl-5-methylene- (9CI)

There total 2 articles about Cyclopentanol, 4-ethylidene-2,2-dimethyl-5-methylene- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

(E)-6-bromo-4,4-dimethylocta-1,6-dien-3-ol → 4-ethylidene-2,2-dimethyl-5-methylidenecyclopentan-1-ol (502497-12-3)

Guidance literature:

With potassium carbonate; triphenylphosphine; palladium diacetate; In acetonitrile; at 80 ℃; for 18h;

DOI:10.1002/1522-2675(200210)85:10<3161::AID-HLCA3161>3.0.CO;2-2

Reference yield:

(E)-4-bromo-2,2-dimethylhex-4-enal → 4-ethylidene-2,2-dimethyl-5-methylidenecyclopentan-1-ol (502497-12-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / tetrahydrofuran / -78 - -20 °C

2: 45 percent / Ph₃P; K₂CO₃ / Pd(OAc)2 / acetonitrile / 18 h / 80 °C

With potassium carbonate; triphenylphosphine; palladium diacetate; In tetrahydrofuran; acetonitrile;

DOI:10.1002/1522-2675(200210)85:10<3161::AID-HLCA3161>3.0.CO;2-2

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