Benzene, 1-chloro-2-(2-chloro-1-(4-chlorophenyl)ethyl)-

Base Information

• Chemical Name: Benzene, 1-chloro-2-(2-chloro-1-(4-chlorophenyl)ethyl)-
• CAS No.: 13312-58-8
• Molecular Formula: C14H11 Cl3
• Molecular Weight: 285.6
• Hs Code.: 2903999090
• NSC Number: 63987
• Mol file: 13312-58-8.mol

Synonyms:13312-58-8;Benzene, 1-chloro-2-(2-chloro-1-(4-chlorophenyl)ethyl)-;1-chloro-2-[2-chloro-1-(4-chlorophenyl)ethyl]benzene;NSC 63987;1-Chloro-2-(2-chloro-1-(4-chlorophenyl)ethyl)benzene;NCIOpen2_002881;NSC63987;NSC-63987;1-chloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)-ethane

Chemical Property of Benzene, 1-chloro-2-(2-chloro-1-(4-chlorophenyl)ethyl)-

Chemical Property:

• Vapor Pressure: 1.96E-05mmHg at 25°C
• Boiling Point: 373.2°Cat760mmHg
• Flash Point: 260.3°C
• PSA: 0.00000
• Density: 1.29g/cm³
• LogP: 5.36410
• XLogP3: 5.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 283.992633
• Heavy Atom Count: 17
• Complexity: 224

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C(CCl)C2=CC=C(C=C2)Cl)Cl

Technology Process of Benzene, 1-chloro-2-(2-chloro-1-(4-chlorophenyl)ethyl)-

There total 4 articles about Benzene, 1-chloro-2-(2-chloro-1-(4-chlorophenyl)ethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o,p'-DDT (789-02-6,58633-26-4) → 1-chloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane (13312-58-8) + 1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane (53-19-0,102976-58-9)

Guidance literature:

With sodium tetrahydroborate; In dimethyl sulfoxide;

DOI:10.1021/ac00111a030

Reference yield:

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane (53-19-0,102976-58-9) → 1-chloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane (13312-58-8)

Guidance literature:

With triethylsilane; {Rh(H)[SiMe₂(o-C₆H₄SMe)](PPh₃)₂}[BAr^F₄]; In neat (no solvent); at 80 ℃; for 72h; Inert atmosphere; Schlenk technique;

DOI:10.1039/C8DT03703E

Reference yield:

2-<2-Chlor-phenyl>-2-<4-chlor-phenyl>-aethanol (92291-62-8) → 1-chloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane (13312-58-8)

Guidance literature:

With pyridine; thionyl chloride;

DOI:10.1021/jo01059a110

upstream raw materials:

2-<2-Chlor-phenyl>-2-<4-chlor-phenyl>-aethanol

o,p'-DDT

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane