3-BROMO-2,2,3-TRIFLUOROPROPANOIC ACID 97

Base Information

• Chemical Name: 3-BROMO-2,2,3-TRIFLUOROPROPANOIC ACID 97
• CAS No.: 679-95-8
• Molecular Formula: C3H2BrF3O2
• Molecular Weight: 206.9448
• Hs Code.: 2915907098
• Mol file: 679-95-8.mol

Synonyms:3-BROMO-2,2,3-TRIFLUOROPROPANOIC ACID 97;3-Bromo-2,2,3-trifluoropropanoic acid 97%

Chemical Property of 3-BROMO-2,2,3-TRIFLUOROPROPANOIC ACID 97

Chemical Property:

• Vapor Pressure: 0.268mmHg at 25°C
• Refractive Index: 1.414
• Boiling Point: 188.4°C at 760 mmHg
• PKA: 0.57±0.10(Predicted)
• Flash Point: 67.7°C
• PSA: 37.30000
• Density: 2.016g/cm³
• LogP: 1.39680

Purity/Quality:

99% ^*data from raw suppliers

3-Bromo-2,2,3-trifluoropropanoic acid 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 34
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BROMO-2,2,3-TRIFLUOROPROPANOIC ACID 97

There total 2 articles about 3-BROMO-2,2,3-TRIFLUOROPROPANOIC ACID 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-1,2,2-trifluoroethene (598-73-2,55157-25-0) + sodium cyanide (143-33-9,25596-52-5) → 3-bromo-2,2,3-trifluoro-propionic acid (679-95-8)

Guidance literature:

With water; acetonitrile;

DOI:10.1021/ja01556a067

Reference yield:

1-bromo-1,2,2-trifluoroethene (598-73-2,55157-25-0) + sodium cyanide (143-33-9,25596-52-5) → 3-bromo-2,2,3-trifluoro-propionic acid (679-95-8)

Guidance literature:

unter Druck;

DOI:10.1021/ja01556a067

Reference yield:

3-bromo-2,2,3-trifluoro-propionic acid (679-95-8) + 5-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1H-indole (1034688-78-2) → 3-[5-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1H-indol-1-yl]-2,2,3-trifluoropropanoic acid (1034687-28-9)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 - 140 ℃; for 11h; Microwave irradiation;

upstream raw materials:

1-bromo-1,2,2-trifluoroethene

sodium cyanide

Downstream raw materials:

3-[5-(5-{3-chloro-4-[(1-methylethyl)oxy]phenyl}-1,2,4-oxadiazol-3-yl)-1H-indol-1-yl]-2,2,3-trifluoropropanoic acid

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