Pentane,1,1,5-trichloro-

Base Information

• Chemical Name: Pentane,1,1,5-trichloro-
• CAS No.: 13059-14-8
• Molecular Formula: C5H9 Cl3
• Molecular Weight: 175.485
• Hs Code.: 2903199000
• Mol file: 13059-14-8.mol

Synonyms:1,1,5-Trichloropentane

Chemical Property of Pentane,1,1,5-trichloro-

Chemical Property:

• PSA: 0.00000
• LogP: 3.19920

Purity/Quality:

99.0%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pentane,1,1,5-trichloro-

There total 2 articles about Pentane,1,1,5-trichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1,5-tetrachloropentane (2467-10-9) + toluene (108-88-3,15644-74-3,16713-13-6) → 1,1,5-trichloropentane (13059-14-8) + benzyl chloride (100-44-7)

Guidance literature:

With iron pentacarbonyl; triphenylphosphine; In benzene; at 160 ℃; for 1h; Product distribution; Mechanism; variation of toluene concentration, other metal carbonyls;

DOI:10.1007/BF00958581

Reference yield:

1,1,1,5-tetrachloropentane (2467-10-9) → 1,1,5-trichloropentane (13059-14-8) + 1,1,5,5-Tetrachlor-pentan (17655-64-0)

Guidance literature:

With iron pentacarbonyl; triphenylphosphine; toluene; In benzene; at 139.9 ℃; for 1.5h; Product distribution; Rate constant; other hydrogen donors, other temperatures;

DOI:10.1007/BF00961494

Reference yield:

1,1,5-trichloropentane (13059-14-8) → 1,5-dichloropentane (628-76-2)

Guidance literature:

With tetramethlyammonium chloride; In methanol; water; (electrochemical reduction);

DOI:10.1021/ja00966a058

upstream raw materials:

1,1,1,5-tetrachloropentane

toluene

Downstream raw materials:

1,5-dichloropentane

Refernces

• 1、 Il'inskaya, L. V.,Gasanov, R. G.. "REACTIVITY OF CERTAIN HYDROGEN DONORS AND OLEFINS WITH RESPECT TO α,α-DICHLOROALKYL RADICALS". . p. 1642 - 1647. Retrieved 2007/10/02.