Cobalt, [(1,2,5,6-eta)-1,5-cyclooctadiene][(eta5-1,3-pentadien-1-yl-5- ylidene)phenylborato(1-)-b]-

Base Information

Chemical Name:Cobalt, [(1,2,5,6-eta)-1,5-cyclooctadiene][(eta5-1,3-pentadien-1-yl-5- ylidene)phenylborato(1-)-b]-
CAS No.:69021-83-6
Molecular Formula:C19H13BCo
Molecular Weight:320.188
Hs Code.:

Synonyms:Cobalt, [(1,2,5,6-eta)-1,5-cyclooctadiene][(eta5-1,3-pentadien-1-yl-5- ylidene)phenylborato(1-)-b]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cobalt, [(1,2,5,6-eta)-1,5-cyclooctadiene][(eta5-1,3-pentadien-1-yl-5- ylidene)phenylborato(1-)-b]-

Chemical Property:

PSA：0.00000
LogP:3.00330

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cobalt, [(1,2,5,6-eta)-1,5-cyclooctadiene][(eta5-1,3-pentadien-1-yl-5- ylidene)phenylborato(1-)-b]-

There total 1 articles about Cobalt, [(1,2,5,6-eta)-1,5-cyclooctadiene][(eta5-1,3-pentadien-1-yl-5- ylidene)phenylborato(1-)-b]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.2%

: cobalt(III) acetylacetonate

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

: 31732-32-8
1-phenyl-1-boracyclohexa-2,5-diene

: 69021-83-6
(η-1,5-Cyclooctadien){1-6-η-(1-phenylborinato)}cobalt

Guidance literature:: With magnesium; In tetrahydrofuran; addn. of Co(acac)3 at 65°C in 3 min, reflux; reagent: Mg activated with anthracene; vac. distn., dissoln. of the residue in pentane, filtration (G3-glassfilter), crystn. (-80°C);
DOI:10.1002/hlca.19840670630

Reference yield: 96.0%

: 69021-83-6
(η-1,5-Cyclooctadien){1-6-η-(1-phenylborinato)}cobalt

: 501-65-5
diphenyl acetylene

: 85025-99-6
(1-phenylborinato)(tetraphenylcyclobutadiene)cobalt

Guidance literature:: In neat (no solvent); under N2, mixt. of educts heated at 180°C for 3 h; chromd. (Al2O3 deactivated with 7% H2O, pentane/CH2Cl2), concd., crystd. from CH2Cl2/pentane; elem. anal.;
DOI:10.1016/0022-328X(83)80020-5

Reference yield: 9.0%

: 503-17-3
dimethylacetylene

: 69021-83-6
(η-1,5-Cyclooctadien){1-6-η-(1-phenylborinato)}cobalt

: 85026-01-3
(tetramethylcyclobutadiene)(1-phenylborinato)cobalt

: 85051-27-0
Co2(1-phenylborinato)2(μ-tetramethylcyclobutadiene)

: 87-85-4
Hexamethylbenzene

Guidance literature:: In 1,2,5-trimethyl-benzene; under N2, educts heated in mesitylene at 150°C for 7 h; evapd. in vac., chromd. (Al2O3 deactivated with 7% H2O, pentane/CH2Cl2), crystd. from pentane; elem. anal.;
DOI:10.1016/0022-328X(83)80020-5