3,5-DINITROBENZOIC ACID, POTASSIUM SALT MIXED

Base Information

• Chemical Name: 3,5-DINITROBENZOIC ACID, POTASSIUM SALT MIXED
• CAS No.: 16345-42-9
• Molecular Formula: C7H4 N2 O6 . K
• Molecular Weight: 250.21
• Hs Code.: 2916399090
• Mol file: 16345-42-9.mol

Synonyms:Benzoicacid, 3,5-dinitro-, potassium salt (8CI,9CI); 3,5-Dinitrobenzoic acid potassiumsalt; Potassium 3,5-dinitrobenzoate

Chemical Property of 3,5-DINITROBENZOIC ACID, POTASSIUM SALT MIXED

Chemical Property:

• PSA: 131.77000
• LogP: 0.91290

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-DINITROBENZOIC ACID, POTASSIUM SALT MIXED

There total 1 articles about 3,5-DINITROBENZOIC ACID, POTASSIUM SALT MIXED which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dinitrobenzoic acid (99-34-3) → 3,5-dinitrobenzoic acid potassium salt (16345-42-9)

Guidance literature:

With potassium carbonate; In water; acetonitrile; at 20 ℃;

DOI:10.1021/cg500883w

Reference yield: 100.0%

3,5-dinitrobenzoic acid potassium salt (16345-42-9) → 3,5-dinitrobenzoyl azide (42444-51-9)

Guidance literature:

With sodium azide; tetrabutylammomium bromide; O-phenyl phosphorodichloridate; In dichloromethane; for 1.5h; Ambient temperature;

Reference yield: 99.0%

[bis(acetato)(2,6-pyridinedicarboxaldehydebis(1-pyrenemethylimine))zinc(II)] monohydrate + 3,5-dinitrobenzoic acid potassium salt (16345-42-9) → [bis(3,5-dinitrophenylacetato)(2,6-pyridinedicarboxaldehydebis(1-pyrenemethylimine))zinc(II)]

Guidance literature:

In methanol; under Ar, 2 equiv. of K-salt, stirring at room temp. for 3 h; ppt. was filtered off, dried, elem. anal.;

upstream raw materials:

3,5-dinitrobenzoic acid

Downstream raw materials:

3,5-dinitrobenzoyl azide

benzoic-3,5-dinitrobenzoic anhydride

[Cu(2-(4'-pyridyl)-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide)2(3,5-dinitrobenzoato)2(H₂O)2]

[Cu(2-(3'-pyridyl)-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide)2(3,5-dinitrobenzoato)2]