1-Cyclohexyl-but-3-EN-1-OL

Base Information

• Chemical Name: 1-Cyclohexyl-but-3-EN-1-OL
• CAS No.: 69036-26-6
• Molecular Formula: C10H18O
• Molecular Weight: 154.252
• DSSTox Substance ID: DTXSID20449119
• Nikkaji Number: J569.985A
• Mol file: 69036-26-6.mol

Synonyms:1-CYCLOHEXYL-BUT-3-EN-1-OL;69036-26-6;1-cyclohexyl-3-buten-1-ol;SCHEMBL420093;DTXSID20449119;MQLWBRPBWCWNPI-UHFFFAOYSA-N;AKOS010638160

Chemical Property of 1-Cyclohexyl-but-3-EN-1-OL

Chemical Property:

• PSA: 20.23000
• LogP: 2.50370
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 154.135765193
• Heavy Atom Count: 11
• Complexity: 114

Purity/Quality:

99% ^*data from raw suppliers

1-CYCLOHEXYL-BUT-3-EN-1-OL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCC(C1CCCCC1)O

Technology Process of 1-Cyclohexyl-but-3-EN-1-OL

There total 117 articles about 1-Cyclohexyl-but-3-EN-1-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

potassium trifluoro(prop-1-en-2-yl)borate + cyclohexanecarbaldehyde (2043-61-0) → 1-cyclohexyl-3-buten-1-ol (69036-26-6)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In dichloromethane; water; at 20 ℃; for 0.25h;

DOI:10.1021/ol026619i

Reference yield: 97.0%

allyltrimethoxysilane (2551-83-9) + cyclohexanecarbaldehyde (2043-61-0) → 1-cyclohexyl-3-buten-1-ol (69036-26-6)

Guidance literature:

allyltrimethoxysilane; cyclohexanecarbaldehyde; With tetrabutylammonium triphenyldifluorosilicate; copper(l) chloride; In tetrahydrofuran; at 20 ℃; for 2.5h;

With hydrogenchloride; In tetrahydrofuran; methanol; Further stages.;

DOI:10.1021/ja0262582

Reference yield: 96.0%

allyl bromide (106-95-6) + cyclohexanecarbaldehyde (2043-61-0) → 1-cyclohexyl-3-buten-1-ol (69036-26-6)

Guidance literature:

With hydrogenchloride; antimony; In water; for 24h;

DOI:10.1139/cjc-79-11-1536

upstream raw materials:

allyldibutyltin chloride

cyclohexanecarbaldehyde

2-(prop-2-en-1-yloxy)oxane

1-Cyclohexyl-1-(trimethylsilyloxy)but-3-ene

Downstream raw materials:

(3,5-Dinitro-phenyl)-carbamic acid (R)-1-cyclohexyl-but-3-enyl ester

(3,5-Dinitro-phenyl)-carbamic acid (S)-1-cyclohexyl-but-3-enyl ester

(R)-<(1R)-1-cyclohexyl-3-buten-1-yl> α-methoxy-α-(trifluoromethyl)phenylacetate

(S)-1-cyclohexylbut-3-enyl 3,3,3-trifluoro-2-methoxy-2-phenylpropanoate