6-CHLORO-2,3-DIAMINOTOLUENE

Base Information

• Chemical Name: 6-CHLORO-2,3-DIAMINOTOLUENE
• CAS No.: 673487-36-0
• Molecular Formula: C7H9ClN2
• Molecular Weight: 156.615
• Hs Code.: 2921590090
• Mol file: 673487-36-0.mol

Synonyms:6-CHLORO-2,3-DIAMINOTOLUENE

Chemical Property of 6-CHLORO-2,3-DIAMINOTOLUENE

Chemical Property:

• Melting Point: 46-47 °C(Solv: benzene (71-43-2); ligroine (8032-32-4))
• Boiling Point: 305.6±37.0 °C(Predicted)
• PKA: 3.65±0.10(Predicted)
• PSA: 52.04000
• Density: 1.281±0.06 g/cm3(Predicted)
• LogP: 2.97520

Purity/Quality:

99%, ^*data from raw suppliers

6-Chloro-2,3-diaminotoluene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-CHLORO-2,3-DIAMINOTOLUENE

There total 4 articles about 6-CHLORO-2,3-DIAMINOTOLUENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloro-2-methyl-6-nitrobenzenamine (51123-59-2) → 4-chloro-3-methylbenzene-1,2-diamine (673487-36-0)

Guidance literature:

With ethanol; ammonium chloride; zinc;

Reference yield:

6-chloro-2,3-dinitro-toluene (290353-56-9) → 4-chloro-3-methylbenzene-1,2-diamine (673487-36-0)

Guidance literature:

With hydrogenchloride; tin; tin(ll) chloride;

Reference yield:

6-chloro-2-nitrotoluene (83-42-1) → 4-chloro-3-methylbenzene-1,2-diamine (673487-36-0)

Guidance literature:

Multi-step reaction with 3 steps

1: HNO₃+H₂SO₄ / 20 °C / dann bei 70-80grad

2: alcoholic ammonia

3: zinc; ammonium chloride; diluted alcohol

With ethanol; sulfuric acid; ammonium chloride; ammonia; nitric acid; zinc;

upstream raw materials:

3-chloro-2-methyl-6-nitrobenzenamine

6-chloro-2,3-dinitro-toluene

6-chloro-2-nitrotoluene

2-methylchlorobenzene

Downstream raw materials:

(S)-(2-(6-chloro-7-methyl-1H-benzo[d]imidazol-2-yl)-2-methylpyrrolidin-1-yl)(5-methoxy-2-(2H-1,2,3-triazol-2-yl)phenyl)methanone

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