Carbamic acid, [1-(aminomethyl)-2-(methylamino)-2-oxoethyl]-, 1,1-

Base Information

Chemical Name:Carbamic acid, [1-(aminomethyl)-2-(methylamino)-2-oxoethyl]-, 1,1-
CAS No.:675601-04-4
Molecular Formula:C9H19N3O3
Molecular Weight:217.27
Hs Code.:
Mol file:675601-04-4.mol

Synonyms:Carbamic acid, [1-(aminomethyl)-2-(methylamino)-2-oxoethyl]-, 1,1-

Suppliers and Price of Carbamic acid, [1-(aminomethyl)-2-(methylamino)-2-oxoethyl]-, 1,1-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [1-(aminomethyl)-2-(methylamino)-2-oxoethyl]-, 1,1-

Chemical Property:

Boiling Point:411.7±40.0 °C(Predicted)
PKA:10.62±0.46(Predicted)
PSA：93.45000
Density:1.089±0.06 g/cm3(Predicted)
LogP:1.06650

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, [1-(aminomethyl)-2-(methylamino)-2-oxoethyl]-, 1,1-

There total 3 articles about Carbamic acid, [1-(aminomethyl)-2-(methylamino)-2-oxoethyl]-, 1,1- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 675601-02-2
benzyl {2-[(tert-butoxycarbonyl)amino]-3-(methylamino)-3-oxopropyl}carbamate

: 675601-04-4
3-amino-N²-(tert-butoxycarbonyl)-N-methylalaninamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 50 ℃; for 4h; under 2585.81 Torr;

Reference yield:

: 76387-70-7
(S)-3-amino-2-tert-butoxycarbonylaminopropionic acid

: 675601-04-4
3-amino-N²-(tert-butoxycarbonyl)-N-methylalaninamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; potassium hydroxide / tetrahydrofuran; water / 16 h / 0 - 20 °C

2.1: HATU / N,N-dimethyl-formamide / 2 h

2.2: 16 h

3.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 50 °C / 2585.81 Torr

With palladium 10% on activated carbon; hydrogen; potassium carbonate; HATU; potassium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 65710-57-8,81306-93-6
3-{[(benzyloxy)carbonyl]amino}-N-(tert-butoxycarbonyl)-L-alanine

: 675601-04-4
3-amino-N²-(tert-butoxycarbonyl)-N-methylalaninamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: HATU / N,N-dimethyl-formamide / 2 h

1.2: 16 h

2.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 50 °C / 2585.81 Torr

With palladium 10% on activated carbon; hydrogen; HATU; In methanol; N,N-dimethyl-formamide;