1H-1,2,4-Triazole-3-carboxylic acid,5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-,methyl ester

Base Information

Chemical Name:1H-1,2,4-Triazole-3-carboxylic acid,5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-,methyl ester
CAS No.:676457-40-2
Molecular Formula:C16H10Cl3N3O2
Molecular Weight:382.633
Hs Code.:
Mol file:676457-40-2.mol

Synonyms:1H-1,2,4-Triazole-3-carboxylic acid,5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-,methyl ester

Suppliers and Price of 1H-1,2,4-Triazole-3-carboxylic acid,5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-,methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-1,2,4-Triazole-3-carboxylic acid,5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-,methyl ester

Chemical Property:

PSA：57.01000
LogP:4.68110

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-1,2,4-Triazole-3-carboxylic acid,5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-,methyl ester

There total 9 articles about 1H-1,2,4-Triazole-3-carboxylic acid,5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-,methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: tert-butyl 2-(2,4-dichlorophenyl)diazene-1-carboxylate

: 76862-09-4
methyl N-(4-chlorobenzylidene)glycinate

: 3-(4-Chlorophenyl)-1-(2,4-dichlorophenyl)-1H-1,2,4-triazole

: 676457-40-2
methyl 5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-1H-1,2,4-triazole-3-carboxylate

Guidance literature:: tert-butyl 2-(2,4-dichlorophenyl)diazene-1-carboxylate; methyl N-(4-chlorobenzylidene)glycinate; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at -15 ℃; for 0.75h; Molecular sieve; Inert atmosphere;

With manganese(IV) oxide; In acetonitrile; at 20 ℃; for 4h;

With trifluoroacetic acid; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2015.04.078

Reference yield: 30.0%

: 91396-09-7
dimethyl [(4-chlorobenzoyl)amino]malonate

: 554-00-7,51908-09-9
2,4-Dichloroaniline

: 676457-40-2
methyl 5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-1H-1,2,4-triazole-3-carboxylate

Guidance literature:: 2,4-Dichloroaniline; With hydrogenchloride; sodium nitrite; In water; acetic acid; at 0 ℃; for 0.25h;

dimethyl [(4-chlorobenzoyl)amino]malonate; In water; acetic acid; acetone; at 0 ℃;

With potassium carbonate; In water; acetic acid; acetone; at 0 ℃; for 0.5h;