1,6-Naphthyridin-2(1H)-one,5,6,7,8-tetrahydro-(9CI)

Base Information

• Chemical Name: 1,6-Naphthyridin-2(1H)-one,5,6,7,8-tetrahydro-(9CI)
• CAS No.: 676994-64-2
• Molecular Formula: C8H10N2O
• Molecular Weight: 150.18
• Hs Code.: 2933990090
• Mol file: 676994-64-2.mol

Synonyms:1,6-Naphthyridin-2(1H)-one,5,6,7,8-tetrahydro-(9CI);5,6,7,8-TETRAHYDRO-1,6-NAPHTHYRIDIN-2(1H)-ONE;5,6,7,8-Tetrahydro-[1,6]naphthyridin-2-ol

Chemical Property of 1,6-Naphthyridin-2(1H)-one,5,6,7,8-tetrahydro-(9CI)

Chemical Property:

• Vapor Pressure: 2.57E-08mmHg at 25°C
• Refractive Index: 1.597
• Boiling Point: 450.8oC at 760 mmHg
• PKA: 12.60±0.20(Predicted)
• Flash Point: 222.9oC
• PSA: 45.15000
• Density: 1.22g/cm3
• LogP: 0.76170
• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

5,6,7,8-Tetrahydro-1,6-naphthyridin-2(1H)-one 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,6-Naphthyridin-2(1H)-one,5,6,7,8-tetrahydro-(9CI)

There total 2 articles about 1,6-Naphthyridin-2(1H)-one,5,6,7,8-tetrahydro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

→ 1,2,5,6,7,8-hexahydro-1,6-naphthyridin-2-one (676994-64-2)

Guidance literature:

Reference yield:

6-benzyl-5,6,7,8-tetrahydro-[1,6]-naphthyridin-2(1H)-one (601514-58-3) → 1,2,5,6,7,8-hexahydro-1,6-naphthyridin-2-one (676994-64-2)

Guidance literature:

With hydrogen; acetic acid; palladium 10% on activated carbon; at 20 ℃; for 38h; under 3102.97 Torr;

Reference yield:

1,2,5,6,7,8-hexahydro-1,6-naphthyridin-2-one (676994-64-2) + [4-(3-chloro-5-cyano-phenoxy)-3-methyl-1H-pyrazol-5-yl]acetic acid (676994-54-0) → C21H18ClN5O3 (676994-47-1)

Guidance literature:

upstream raw materials:

6-benzyl-5,6,7,8-tetrahydro-[1,6]-naphthyridin-2(1H)-one

Downstream raw materials:

C₂₁H₁₈ClN₅O₃

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