Cyclohexanecarboxylic acid, 3,4-dimethyl- (9CI)

Base Information

• Chemical Name: Cyclohexanecarboxylic acid, 3,4-dimethyl- (9CI)
• CAS No.: 681448-23-7
• Molecular Formula: C₉H₁₆O₂
• Molecular Weight: 156.225
• Mol file: 681448-23-7.mol

Synonyms:Cyclohexanecarboxylic acid, 3,4-dimethyl- (9CI)

Chemical Property of Cyclohexanecarboxylic acid, 3,4-dimethyl- (9CI)

Chemical Property:

• Boiling Point: 155.5 - 155.8 °C (20.5 mmHg)
• PSA: 37.30000
• LogP: 2.14330

Purity/Quality:

99% ^*data from raw suppliers

3,4-dimethylcyclohexane-1-carboxylicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxylic acid, 3,4-dimethyl- (9CI)

There total 5 articles about Cyclohexanecarboxylic acid, 3,4-dimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dimethylbenzoic acid (619-04-5) → 3,4-dimethyl-cyclohexanecarboxylic acid (681448-23-7)

Guidance literature:

With acetic acid; platinum; Hydrogenation;

DOI:10.1021/ja01169a024

Reference yield:

3,4-dimethylbenzoic acid (619-04-5) → 3,4-dimethyl-cyclohexanecarboxylic acid (681448-23-7)

Guidance literature:

With i-Amyl alcohol; sodium; Trennung ihres Anilids oder durch ihre Bestaendigkeit gegen KMnO₄;

DOI:10.1108/03684920110363914

Reference yield:

1,2,4-Trimethylbenzene (95-63-6) → 3,4-dimethyl-cyclohexanecarboxylic acid (681448-23-7)

Guidance literature:

Multi-step reaction with 2 steps

1: diluted nitric acid

2: sodium; isoamyl alcohol / Trennung ihres Anilids oder durch ihre Bestaendigkeit gegen KMnO₄

With i-Amyl alcohol; nitric acid; sodium;

DOI:10.1108/03684920110363914

upstream raw materials:

3,4-dimethylbenzoic acid

i-Amyl alcohol

1,2,4-Trimethylbenzene