3aH-Cyclopent[d]isoxazole-3a-methanol,3-cyclopropylhexahydro-2-methyl-,(3R,3aR,6aR)-(9CI)

Base Information

Chemical Name:3aH-Cyclopent[d]isoxazole-3a-methanol,3-cyclopropylhexahydro-2-methyl-,(3R,3aR,6aR)-(9CI)
CAS No.:607405-13-0
Molecular Formula:C11H19NO2
Molecular Weight:197.27
Hs Code.:
Mol file:607405-13-0.mol

Synonyms:3aH-Cyclopent[d]isoxazole-3a-methanol,3-cyclopropylhexahydro-2-methyl-,(3R,3aR,6aR)-(9CI)

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Chemical Property of 3aH-Cyclopent[d]isoxazole-3a-methanol,3-cyclopropylhexahydro-2-methyl-,(3R,3aR,6aR)-(9CI)

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Technology Process of 3aH-Cyclopent[d]isoxazole-3a-methanol,3-cyclopropylhexahydro-2-methyl-,(3R,3aR,6aR)-(9CI)

There total 2 articles about 3aH-Cyclopent[d]isoxazole-3a-methanol,3-cyclopropylhexahydro-2-methyl-,(3R,3aR,6aR)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6140-65-4
1-cyclopentene-1-carboxaldehyde

: 86209-99-6,65194-05-0
c-cyclopropyl-N-methylnitrone

: 607405-13-0
[(3S,3aS,6aS)-3-cyclopropyl-2-methylhexahydro-3aH-cyclopenta[d]isoxazol-3a-yl]methanol

: 607405-13-0
[(3R,3aR,6aR)-3-cyclopropyl-2-methylhexahydro-3aH-cyclopenta[d]isoxazol-3a-yl]methanol

Guidance literature:: 1-cyclopentene-1-carboxaldehyde; c-cyclopropyl-N-methylnitrone; With chiral pyrrolidine derivative dihydrochloride; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.5h; Further stages. Title compound not separated from byproducts.;
DOI:10.1002/ejoc.200300172

Reference yield:

: 6140-65-4
1-cyclopentene-1-carboxaldehyde

: 86209-99-6,65194-05-0
c-cyclopropyl-N-methylnitrone

: 607405-13-0
[(3S,3aS,6aS)-3-cyclopropyl-2-methylhexahydro-3aH-cyclopenta[d]isoxazol-3a-yl]methanol

: 607405-13-0
[(3R,3aR,6aR)-3-cyclopropyl-2-methylhexahydro-3aH-cyclopenta[d]isoxazol-3a-yl]methanol

Guidance literature:: 1-cyclopentene-1-carboxaldehyde; c-cyclopropyl-N-methylnitrone; With chiral pyrrolidine derivative dihydrochloride; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.5h; Further stages. Title compound not separated from byproducts.;
DOI:10.1002/ejoc.200300172