(S,RP)-PH-DIAPHOX

Base Information

Chemical Name:(S,RP)-PH-DIAPHOX
CAS No.:685139-79-1
Molecular Formula:C23H26N3OP
Molecular Weight:391.45
Hs Code.:
Mol file:685139-79-1.mol

Synonyms:(S,RP)-PH-DIAPHOX

Suppliers and Price of (S,RP)-PH-DIAPHOX

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(S,RP)-PH-DIAPHOX 95.00%
5MG
$ 502.82

Total 5 raw suppliers

Chemical Property of (S,RP)-PH-DIAPHOX

Chemical Property:

Boiling Point:approximate 130℃
PSA：52.33000
LogP:5.17470

Purity/Quality:

95% ^*data from raw suppliers

(S,RP)-PH-DIAPHOX 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (S,RP)-PH-DIAPHOX

There total 8 articles about (S,RP)-PH-DIAPHOX which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 685139-78-0
(2R)-N²-benzyl-N¹,N⁴-diphenyl-butane-1,2,4-triamine

: 685139-79-1
(S,R(P))-DIAPHOX

Guidance literature:: With triethylamine; phosphorus trichloride; In toluene; at -78 - 20 ℃;
DOI:10.1002/adsc.200505149

Reference yield:

: 685139-83-7
(S)-8-Benzyl-2,7-diphenyl-2,7,8-triaza-1-phospha-bicyclo[3.2.1]octane

: (S)-8-Benzyl-2,7-diphenyl-2,7,8-triaza-1-phospha-bicyclo[3.2.1]octane 1-oxide

: ((S)-3-Benzyl-2-oxo-1-phenyl-2λ⁵-[1,3,2]diazaphosphinan-4-ylmethyl)-phenyl-amine

: 685139-79-1
(S,R(P))-DIAPHOX

Guidance literature:: With water; silica gel; In ethyl acetate; at 20 ℃; for 20h;
DOI:10.1021/ja031792a

Reference yield:

: 62-53-3
aniline

: 685139-79-1
(S,R(P))-DIAPHOX

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethylformamide / 3 h / 20 °C

1.2: 87 percent / WSCI / dimethylformamide / 24 h / 20 °C

2.1: H₂ / Pd/C / dimethylformamide; propan-2-ol / 2 h / 20 °C

3.1: 97 percent / Et₃N / tetrahydrofuran / 1 h / 0 °C

4.1: 72 percent / LAH / tetrahydrofuran / 13 h / Heating

5.1: 60 percent / phosphorous trichloride; Et₃N / toluene / -78 - 20 °C

With lithium aluminium tetrahydride; hydrogen; triethylamine; phosphorus trichloride; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
DOI:10.1002/adsc.200505149