Bicyclo[2.2.1]heptane-2,6-diol, monoacetate, (1S,2S,4R,6S)- (9CI)

Base Information

Chemical Name:Bicyclo[2.2.1]heptane-2,6-diol, monoacetate, (1S,2S,4R,6S)- (9CI)
CAS No.:615249-16-6
Molecular Formula:C₉H₁₄O₃
Molecular Weight:170.208
Hs Code.:
Mol file:615249-16-6.mol

Synonyms:Bicyclo[2.2.1]heptane-2,6-diol, monoacetate, (1S,2S,4R,6S)- (9CI)

Suppliers and Price of Bicyclo[2.2.1]heptane-2,6-diol, monoacetate, (1S,2S,4R,6S)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[2.2.1]heptane-2,6-diol, monoacetate, (1S,2S,4R,6S)- (9CI)

Chemical Property:

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Technology Process of Bicyclo[2.2.1]heptane-2,6-diol, monoacetate, (1S,2S,4R,6S)- (9CI)

There total 26 articles about Bicyclo[2.2.1]heptane-2,6-diol, monoacetate, (1S,2S,4R,6S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: endo-5-norbornen-2-yl acetate

: 615249-16-6
2-endo-6-exo-6-hydroxybicyclo[2.2.1]heptan-2-yl acetate

: 615249-15-5
2-endo-6-exo-6-hydroxybicyclo[2.2.1]heptan-2-yl acetate

Guidance literature:: endo-5-norbornen-2-yl acetate; With borane-THF; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; water; at 0 ℃; for 0.833333h; Overall yield = 7.79 g;
DOI:10.1016/j.tet.2013.09.071

Reference yield:

: 154278-40-7
(1S,2S,4S)-bicyclo[2.2.1]hept-5-en-2-yl acetate

: 615249-16-6
Acetic acid (1S,2S,4R,6S)-6-hydroxy-bicyclo[2.2.1]hept-2-yl ester

: Acetic acid (1S,2S,4S,5R)-5-hydroxy-bicyclo[2.2.1]hept-2-yl ester

Guidance literature:: (1S,2S,4S)-bicyclo[2.2.1]hept-5-en-2-yl acetate; With borane-THF; In tetrahydrofuran; at 0 ℃; for 1h;

With sodium hydroxide; dihydrogen peroxide; for 0.5h; Title compound not separated from byproducts;
DOI:10.1002/anie.200351744

Reference yield:

: bicyclo[2.2.1]hept-5-en-2-yl acetate

: 615249-16-6
C₉H₁₄O₃

: C₉H₁₄O₃

Guidance literature:: bicyclo[2.2.1]hept-5-en-2-yl acetate; With borane-THF; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;

With sodium perborate tetrahydrate; water; at 20 ℃;
DOI:10.1016/j.bmc.2010.04.081