Technology Process of Tricyclo[8.4.1.1(3,8)]hexadeca-3,5,7,10,12,14-hexaene-2,9-dione, anti-
There total 7 articles about Tricyclo[8.4.1.1(3,8)]hexadeca-3,5,7,10,12,14-hexaene-2,9-dione, anti- which
guide to synthetic route it.
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synthetic route:
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7082-43-1,104713-91-9,104713-92-0
2r,7c;9t,14t-Dimethano-cyclotetradeca-2,4,6,9,11,13-hexaen-1,8-dion
- Guidance literature:
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With
dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
In
dichloromethane;
at -78 ℃;
for 1h;
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7082-43-1,104713-91-9,104713-92-0
2r,7c;9t,14t-Dimethano-cyclotetradeca-2,4,6,9,11,13-hexaen-1,8-dion
- Guidance literature:
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Multi-step reaction with 3 steps
1: 90 percent / Br2 / CH2Cl2 / Ambient temperature
2: 85 percent / AgNO3, H2O / acetone / 0.5 h / Ambient temperature
3: 85 percent / DMSO/TFAA/NEt3 / CH2Cl2 / 1 h / -78 °C
With
water; bromine; silver nitrate; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
In
dichloromethane; acetone;
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-
7082-43-1,104713-91-9,104713-92-0
2r,7c;9t,14t-Dimethano-cyclotetradeca-2,4,6,9,11,13-hexaen-1,8-dion
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / AgNO3, H2O / acetone / 0.5 h / Ambient temperature
2: 85 percent / DMSO/TFAA/NEt3 / CH2Cl2 / 1 h / -78 °C
With
water; silver nitrate; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
In
dichloromethane; acetone;