Benzeneacetaldehyde, alpha-ethylidene-4-fluoro-, (alphaE)- (9CI)

Base Information

Chemical Name:Benzeneacetaldehyde, alpha-ethylidene-4-fluoro-, (alphaE)- (9CI)
CAS No.:694513-38-7
Molecular Formula:C10H9FO
Molecular Weight:164.1762632
Hs Code.:
Mol file:694513-38-7.mol

Synonyms:Benzeneacetaldehyde, alpha-ethylidene-4-fluoro-, (alphaE)- (9CI)

Suppliers and Price of Benzeneacetaldehyde, alpha-ethylidene-4-fluoro-, (alphaE)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Benzeneacetaldehyde, alpha-ethylidene-4-fluoro-, (alphaE)- (9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:: 99%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzeneacetaldehyde, alpha-ethylidene-4-fluoro-, (alphaE)- (9CI)

There total 3 articles about Benzeneacetaldehyde, alpha-ethylidene-4-fluoro-, (alphaE)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-73-9,4170-30-3
trans-Crotonaldehyde

: 118798-76-8
tris(4-fluorophenyl)bismuth dichloride

: 694513-38-7
(E)-2-(4-Fluoro-phenyl)-but-2-enal

: 694513-38-7
(Z)-2-(4-Fluoro-phenyl)-but-2-enal

Guidance literature:: With tributylphosphine; N-ethyl-N,N-diisopropylamine; In dichloromethane; tert-butyl alcohol; at 25 ℃; Title compound not separated from byproducts;
DOI:10.1021/ja048987i

Reference yield:

: 123-73-9,4170-30-3
trans-Crotonaldehyde

: 118798-76-8
tris(4-fluorophenyl)bismuth dichloride

: 694513-38-7
(E)-2-(4-Fluoro-phenyl)-but-2-enal

: 694513-38-7
(Z)-2-(4-Fluoro-phenyl)-but-2-enal

Guidance literature:: With tributylphosphine; N-ethyl-N,N-diisopropylamine; In dichloromethane; tert-butyl alcohol; at 25 ℃; Title compound not separated from byproducts;
DOI:10.1021/ja048987i

Reference yield:

: 4-(4-fluorophenyl)-4-vinyl-1,3-dioxolan-2-one

: 694513-38-7
C₁₀H₉FO

: C₂₀H₁₈F₂O₂

Guidance literature:: With [1,2-bis-(phenylsulfinyl)ethane]palladium(II) acetate; bis[2-(diphenylphosphino)phenyl] ether; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.7b12608