5H-6,7a-Methano-1H,3H-pyrrolo[1,2-c]oxazol-3-one,dihydro-(9CI)

Base Information

Chemical Name:5H-6,7a-Methano-1H,3H-pyrrolo[1,2-c]oxazol-3-one,dihydro-(9CI)
CAS No.:637740-07-9
Molecular Formula:C7H9NO2
Molecular Weight:139.15
Hs Code.:
Mol file:637740-07-9.mol

Synonyms:5H-6,7a-Methano-1H,3H-pyrrolo[1,2-c]oxazol-3-one,dihydro-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5H-6,7a-Methano-1H,3H-pyrrolo[1,2-c]oxazol-3-one,dihydro-(9CI)

Chemical Property:

Melting Point:29.5 - 31.5 °C
PSA：29.54000
LogP:0.53890

Purity/Quality:

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Technology Process of 5H-6,7a-Methano-1H,3H-pyrrolo[1,2-c]oxazol-3-one,dihydro-(9CI)

There total 1 articles about 5H-6,7a-Methano-1H,3H-pyrrolo[1,2-c]oxazol-3-one,dihydro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 288-32-4
1H-imidazole

: 637740-06-8
1-methanesulfonyloxymethyl-2-azabicyclo[2.1.1]hexane-2-carboxylic acid benzyl ester

: 637740-07-9
3-oxa-5-aza-tricyclo[5.1.1.0^1,5]nonan-4-one

: 637740-10-4
1-imidazol-1-ylmethyl-2-aza-bicyclo[2.1.1]hexane-2-carboxylic acid benzyl ester

Guidance literature:: 1H-imidazole; With n-butyllithium; In hexane; acetonitrile; for 0.25h;

1-methanesulfonyloxymethyl-2-azabicyclo[2.1.1]hexane-2-carboxylic acid benzyl ester; In hexane; acetonitrile; at 40 ℃; for 96h;
DOI:10.1021/jo035199n

Reference yield: 55.0%

: 288-32-4
1H-imidazole

: 637740-07-9
3-oxa-5-aza-tricyclo[5.1.1.0^1,5]nonan-4-one

: 637740-11-5
1-imidazol-1-ylmethyl-2-azabicyclo[2.1.1]hexane

Guidance literature:: 1H-imidazole; With n-butyllithium; In hexane; N,N-dimethyl-formamide; for 0.25h;

3-oxa-5-aza-tricyclo[5.1.1.0^1,5]nonan-4-one; In hexane; N,N-dimethyl-formamide; at 90 ℃; for 144h;
DOI:10.1021/jo035199n