1,2-Oxathiolane,5-ethyl-3-phenyl-,2,2-dioxide,(3R,5R)-(9CI)

Base Information

Chemical Name:1,2-Oxathiolane,5-ethyl-3-phenyl-,2,2-dioxide,(3R,5R)-(9CI)
CAS No.:637775-88-3
Molecular Formula:C₁₁H₁₄O₃S
Molecular Weight:226.296
Hs Code.:
Mol file:637775-88-3.mol

Synonyms:1,2-Oxathiolane,5-ethyl-3-phenyl-,2,2-dioxide,(3R,5R)-(9CI)

Suppliers and Price of 1,2-Oxathiolane,5-ethyl-3-phenyl-,2,2-dioxide,(3R,5R)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,2-Oxathiolane,5-ethyl-3-phenyl-,2,2-dioxide,(3R,5R)-(9CI)

Chemical Property:

Melting Point:106 °C
PSA：51.75000
LogP:3.33720

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1,2-Oxathiolane,5-ethyl-3-phenyl-,2,2-dioxide,(3R,5R)-(9CI)

There total 1 articles about 1,2-Oxathiolane,5-ethyl-3-phenyl-,2,2-dioxide,(3R,5R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-1-phenyl-3-pentene-1-sulfonic acid

: (3R,5S)-5-ethyl-3-phenyl-1,2-oxathiolane 2,2-dioxide

: 637775-88-3
(3R,5R)-5-ethyl-3-phenyl-1,2-oxathiolane 2,2-dioxide

: (3R,6R)-6-Methyl-3-phenyl-[1,2]oxathiane 2,2-dioxide

: (3R,6S)-6-Methyl-3-phenyl-[1,2]oxathiane 2,2-dioxide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 16h; Heating;
DOI:10.1002/ejoc.200300342

Reference yield:

: 637775-88-3
(3R,5R)-5-ethyl-3-phenyl-1,2-oxathiolane 2,2-dioxide

: (1R,3S)-3-Azido-1-phenyl-pentane-1-sulfonic acid

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 60 ℃; for 2h;
DOI:10.1055/s-2004-831256

Reference yield:

: 637775-88-3
(3R,5R)-5-ethyl-3-phenyl-1,2-oxathiolane 2,2-dioxide

: isopropyl (1R,3S)-3-tert-butoxycarbonylamino-1-phenylpentanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃; NH₄Cl / dimethylformamide / 2 h / 60 °C

2: 154 mg / CH₂Cl₂ / 2 h / Heating

3: 86 percent / H₂ / Pd/C / ethyl acetate / 20 h / 20 °C

With sodium azide; hydrogen; ammonium chloride; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1055/s-2004-831256