4-chloro-N-cyclohexylideneaniline

Base Information

• Chemical Name: 4-chloro-N-cyclohexylideneaniline
• CAS No.: 36132-64-6
• Molecular Formula: C12H14 Cl N
• Molecular Weight: 207.703
• Mol file: 36132-64-6.mol

Synonyms:4'-Chlorophenyliminocyclohexane;Aniline, p-chloro-N-cyclohexylidene-; N-Cyclohexylidene-p-chloroaniline; NSC13061

Chemical Property of 4-chloro-N-cyclohexylideneaniline

Chemical Property:

• Vapor Pressure: 0.00207mmHg at 25°C
• Boiling Point: 299.9°C at 760 mmHg
• Flash Point: 135.2°C
• Density: 1.13g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-chloro-N-cyclohexylideneaniline

There total 3 articles about 4-chloro-N-cyclohexylideneaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + 4-chloro-aniline (106-47-8) → N-(cyclohexylidine)-4-chloro-aniline (36132-64-6)

Guidance literature:

With acetic acid; In toluene; Heating;

Reference yield:

C12H16ClN → N-(cyclohexylidine)-4-chloro-aniline (36132-64-6)

Guidance literature:

With [bis(acetoxy)iodo]benzene; caesium carbonate; In methanol; at 0 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/acs.orglett.9b00559

Reference yield:

→ N-(cyclohexylidine)-4-chloro-aniline (36132-64-6)

Guidance literature:

Cyclohexanondiethylacetal, p-Chloranilin;

upstream raw materials:

cyclohexanone

4-chloro-aniline

Downstream raw materials:

[1-(4-Chloro-phenylamino)-cyclohexyl]-phosphonic acid dimethyl ester

4-chloro-N-cyclohexylaniline

C₁₆H₁₈ClNO₃S

3',4'-Dichlor-2-oxo-cyclohexancarbanilid