Oxiraneacetaldehyde, 3-ethyl- (9CI)

Base Information

• Chemical Name: Oxiraneacetaldehyde, 3-ethyl- (9CI)
• CAS No.: 641613-25-4
• Molecular Formula: C6H10 O2
• Molecular Weight: 114.144
• Mol file: 641613-25-4.mol

Synonyms:Oxiraneacetaldehyde,3-ethyl- (9CI); 3-Ethyloxirane-2-acetaldehyde

Chemical Property of Oxiraneacetaldehyde, 3-ethyl- (9CI)

Chemical Property:

• PSA: 29.60000
• LogP: 0.75280

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Oxiraneacetaldehyde, 3-ethyl- (9CI)

There total 2 articles about Oxiraneacetaldehyde, 3-ethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-(3-ethyloxiran-2-yl)ethan-1-ol (67663-02-9) → 2-(3-ethyloxiran-2-yl)acetaldehyde (641613-25-4)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.333333h;

DOI:10.1021/acs.joc.9b02378

Reference yield:

3-hexen-1-ol (544-12-7) → 2-(3-ethyloxiran-2-yl)ethan-1-ol (67663-02-9) + 2-(3-ethyloxiran-2-yl)acetaldehyde (641613-25-4)

Guidance literature:

With tert.-butylhydroperoxide; In chloroform; at 70 ℃; for 4h; Reagent/catalyst; chemoselective reaction;

DOI:10.1016/j.catcom.2015.10.022

upstream raw materials:

2-(3-ethyloxiran-2-yl)ethan-1-ol

3-hexen-1-ol

Refernces

• 1、 Fan, Weizheng,Shi, Dongyang,Feng, Bainian. "Immobilizing of oxo-molybdenum complex on cross-linked copolymer and its catalytic activity for epoxidation reactions". . p. 1 - 4. Retrieved 2015/11/10.