4,6-Dioxa-2-azabicyclo[3.2.0]hept-2-ene,7-ethyl-5-methoxy-3-methyl-1-(2-methylpropyl)-,(1R,5S,7R)-rel-(9CI)

Base Information

Chemical Name:4,6-Dioxa-2-azabicyclo[3.2.0]hept-2-ene,7-ethyl-5-methoxy-3-methyl-1-(2-methylpropyl)-,(1R,5S,7R)-rel-(9CI)
CAS No.:647012-62-2
Molecular Formula:C₁₂H₂₁NO₃
Molecular Weight:227.304
Hs Code.:
Mol file:647012-62-2.mol

Synonyms:4,6-Dioxa-2-azabicyclo[3.2.0]hept-2-ene,7-ethyl-5-methoxy-3-methyl-1-(2-methylpropyl)-,(1R,5S,7R)-rel-(9CI)

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Chemical Property of 4,6-Dioxa-2-azabicyclo[3.2.0]hept-2-ene,7-ethyl-5-methoxy-3-methyl-1-(2-methylpropyl)-,(1R,5S,7R)-rel-(9CI)

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Technology Process of 4,6-Dioxa-2-azabicyclo[3.2.0]hept-2-ene,7-ethyl-5-methoxy-3-methyl-1-(2-methylpropyl)-,(1R,5S,7R)-rel-(9CI)

There total 4 articles about 4,6-Dioxa-2-azabicyclo[3.2.0]hept-2-ene,7-ethyl-5-methoxy-3-methyl-1-(2-methylpropyl)-,(1R,5S,7R)-rel-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 647012-62-2
7-exo-ethyl-1-isobutyl-5-methoxy-3-methyl-4,6-dioxa-2-azabicyclo[3.2.0]hept-2-ene

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / 3 h / Heating

2.1: Et₃N / CHCl₃ / 0.25 h / 20 °C

2.2: CHCl₃ / 0.75 h / 20 °C

3.1: 70 percent / phosphorus pentachloride / CHCl₃ / 60 °C

4.1: benzene / 24 h / 10 °C / UV-irradiation

With thionyl chloride; phosphorus pentachloride; triethylamine; In chloroform; benzene;
DOI:10.1021/jo034830h

Reference yield:

: 2-acetylamino-4-methyl-pentanoic acid methyl ester

: 647012-62-2
7-exo-ethyl-1-isobutyl-5-methoxy-3-methyl-4,6-dioxa-2-azabicyclo[3.2.0]hept-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / phosphorus pentachloride / CHCl₃ / 60 °C

2: benzene / 24 h / 10 °C / UV-irradiation

With phosphorus pentachloride; In chloroform; benzene;
DOI:10.1021/jo034830h

Reference yield:

: 2-amino-4-methyl-pentanoic acid methyl ester; hydrochloride

: 647012-62-2
7-exo-ethyl-1-isobutyl-5-methoxy-3-methyl-4,6-dioxa-2-azabicyclo[3.2.0]hept-2-ene

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N / CHCl₃ / 0.25 h / 20 °C

1.2: CHCl₃ / 0.75 h / 20 °C

2.1: 70 percent / phosphorus pentachloride / CHCl₃ / 60 °C

3.1: benzene / 24 h / 10 °C / UV-irradiation

With phosphorus pentachloride; triethylamine; In chloroform; benzene;
DOI:10.1021/jo034830h