3-Acetoxybenzamide

Base Information

Chemical Name:3-Acetoxybenzamide
CAS No.:77719-00-7
Molecular Formula:C₉H₉NO₃
Molecular Weight:179.175
Hs Code.:
NSC Number:123375
DSSTox Substance ID:DTXSID10298476
Wikidata:Q82040307

Synonyms:3-acetoxybenzamide;77719-00-7;m-acetoxybenzamide;NSC123375;SCHEMBL2403571;DTXSID10298476;RAYNCJUZMAVTHF-UHFFFAOYSA-N;NSC-123375

Suppliers and Price of 3-Acetoxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-Acetoxybenzamide

Chemical Property:

Vapor Pressure:0.000286mmHg at 25°C
Boiling Point:322.1°C at 760 mmHg
Flash Point:170.6°C
Density:1.229g/cm³
XLogP3:0.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:179.058243149
Heavy Atom Count:13
Complexity:215

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1=CC=CC(=C1)C(=O)N

Technology Process of 3-Acetoxybenzamide

There total 4 articles about 3-Acetoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 618-49-5
3-hydroxybenzamide

: 108-24-7
acetic anhydride

: 77719-00-7
m-acetoxybenzamide

Guidance literature:: With pyridine; at 0 ℃; for 4h;

Reference yield:

: 16446-73-4
3-(chlorocarbonyl)phenyl acetate

: 77719-00-7
m-acetoxybenzamide

Guidance literature:: With chloroform; ammonia;

Reference yield:

: 99-06-9
3-Carboxyphenol

: 77719-00-7
m-acetoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) thionyl chloride, 2.) ammonium hydroxide / 1.) reflux, 4 h, 2.) 0 deg C

2: 58 percent / pyridine / 4 h / 0 °C

With pyridine; ammonium hydroxide; thionyl chloride;