Cyclopentane, 3-ethylidene-1,1-bis(methoxymethyl)-4-methyl-, (3E)- (9CI)

Base Information

Chemical Name:Cyclopentane, 3-ethylidene-1,1-bis(methoxymethyl)-4-methyl-, (3E)- (9CI)
CAS No.:652154-92-2
Molecular Formula:C12H22O2
Molecular Weight:198.30188
Hs Code.:
Mol file:652154-92-2.mol

Synonyms:Cyclopentane, 3-ethylidene-1,1-bis(methoxymethyl)-4-methyl-, (3E)- (9CI)

Suppliers and Price of Cyclopentane, 3-ethylidene-1,1-bis(methoxymethyl)-4-methyl-, (3E)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopentane, 3-ethylidene-1,1-bis(methoxymethyl)-4-methyl-, (3E)- (9CI)

Chemical Property:

PSA：18.46000
LogP:2.64180

Purity/Quality:

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Technology Process of Cyclopentane, 3-ethylidene-1,1-bis(methoxymethyl)-4-methyl-, (3E)- (9CI)

There total 3 articles about Cyclopentane, 3-ethylidene-1,1-bis(methoxymethyl)-4-methyl-, (3E)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 499128-96-0
(Z)-1,1-bis(methoxymethyl)-4-(1-triethylsilylethylidene)-3-methylcyclopentane

: 652154-92-2
3E-ethylidene-1,1-bis(methoxymethyl)-4-methylcyclopentane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1021/ol027196n

Reference yield: 75.0%

: 499128-86-8
4,4-bis(methoxymethyl)-1-octene-6-yne

: 652154-92-2
3E-ethylidene-1,1-bis(methoxymethyl)-4-methylcyclopentane

Guidance literature:: 4,4-bis(methoxymethyl)-1-octene-6-yne; With n-butyllithium; zirconocene dichloride; In tetrahydrofuran; at -78 - 20 ℃;

With hydrogenchloride; In tetrahydrofuran; for 0.166667h;
DOI:10.1021/ol036031r

Reference yield:

: 428517-22-0
4,4-bis(methoxymethyl)-hept-6-en-1-yne

: 652154-92-2
3E-ethylidene-1,1-bis(methoxymethyl)-4-methylcyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran / 0.5 h / 0 °C

1.2: 89 percent / tetrahydrofuran / 0 - 20 °C

2.1: Cp₂ZrCl₂; n-BuLi / tetrahydrofuran / -78 - 20 °C

2.2: 75 percent / hydrochloric acid / tetrahydrofuran / 0.17 h

With n-butyllithium; zirconocene dichloride; In tetrahydrofuran;
DOI:10.1021/ol036031r