2,6-DIMETHYLTETRALINE

Base Information

• Chemical Name: 2,6-DIMETHYLTETRALINE
• CAS No.: 7524-63-2
• Molecular Formula: C₁₂H₁₆
• Molecular Weight: 160.259
• Mol file: 7524-63-2.mol

Synonyms:2,6-DIMETHYLTETRALINE;1,2,3,4-Tetrahydro-2,6-dimethylnaphthalene;2,6-Dimethyl-1,2,3,4-tetrahydronaphthalene;Naphthalene, 1,2,3,4-tetrahydro-2,6-dimethyl-

Chemical Property of 2,6-DIMETHYLTETRALINE

Chemical Property:

• Melting Point: 20°C
• Refractive Index: 1.5260
• Boiling Point: 246.18°C (estimate)
• PSA: 0.00000
• Density: 0.9410
• LogP: 3.11980

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-DIMETHYLTETRALINE

There total 10 articles about 2,6-DIMETHYLTETRALINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-methyl-4-(p-tolyl)-1-butanol (868748-03-2) → 2,6-dimethyltetralin (7524-63-2,137823-69-9,137823-70-2)

Guidance literature:

With Amberlyst 15; In chlorobenzene; at 200 ℃; for 2h; Solvent; Reagent/catalyst;

DOI:10.1021/op050072g

Reference yield: 76.0%

3-methyl-4-(p-tolyl)-1-butanol (868748-03-2) → 2.6-dimethylnaphthalene (581-42-0) + 2,6-dimethyltetralin (7524-63-2,137823-69-9,137823-70-2)

Guidance literature:

With titanium tetrachloride; In chlorobenzene; at 200 ℃; for 2h; Reagent/catalyst;

DOI:10.1021/op050072g

Reference yield:

2.6-dimethylnaphthalene (581-42-0) → 2,6-dimethyltetralin (7524-63-2,137823-69-9,137823-70-2) + decahydro-2,6-dimethylnaphthalene (1618-22-0)

Guidance literature:

With 1-butyl-1-methylpiperidinium nickel thiotungstate; hydrogen; at 350 ℃; for 10h; under 37503.8 Torr; Autoclave;

DOI:10.1134/S0965544115060110

upstream raw materials:

2.6-dimethylnaphthalene

1,4-dimethylnaphthalene

3-methyl-4-(p-tolyl)-1-butanol

para-bromotoluene

Downstream raw materials:

1,2,4-benzene tricarboxylic acid