TRANS-N,N'-DIACETYLCYCLOHEXANE-1,2-DIAMINE

Base Information

• Chemical Name: TRANS-N,N'-DIACETYLCYCLOHEXANE-1,2-DIAMINE
• CAS No.: 70924-78-6
• Molecular Formula: C₁₀H₁₈N₂O₂
• Molecular Weight: 198.265
• Hs Code.: 2924299090
• Mol file: 70924-78-6.mol

Synonyms:TRANS-N,N'-DIACETYLCYCLOHEXANE-1,2-DIAMINE;TRANS-1,2-BIS(ACETAMIDO)CYCLOHEXANE

Chemical Property of TRANS-N,N'-DIACETYLCYCLOHEXANE-1,2-DIAMINE

Chemical Property:

• Melting Point: 270 °C
• Boiling Point: 469.1±25.0 °C(Predicted)
• PKA: 15.29±0.40(Predicted)
• PSA: 58.20000
• Density: 1.06±0.1 g/cm3(Predicted)
• LogP: 1.35160
• Solubility.: soluble in Methanol

Purity/Quality:

98%,99%, ^*data from raw suppliers

trans-N,N'-Diacetylcyclohexane-1,2-diamine >98.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TRANS-N,N'-DIACETYLCYCLOHEXANE-1,2-DIAMINE

There total 1 articles about TRANS-N,N'-DIACETYLCYCLOHEXANE-1,2-DIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

trans-1,2-Diaminocyclohexane (1121-22-8,1436-59-5,20439-47-8,21436-03-3,41013-43-8,694-83-7) + acetic anhydride (108-24-7) → N,N'-diacetyl-trans-1,2-diaminocyclohexane (54009-70-0,70924-77-5,70924-78-6)

Guidance literature:

In chloroform; for 1h;

DOI:10.3891/acta.chem.scand.50-0938

Reference yield: 100.0%

N,N'-diacetyl-trans-1,2-diaminocyclohexane (54009-70-0,70924-77-5,70924-78-6) → N-((1S,2S)-2-Thioacetylamino-cyclohexyl)-thioacetamide

Guidance literature:

With 2,4-bis<4-(methylthio)phenyl>-1,3,2,4-dithiadiphosphetane 2,4-disulfide; In toluene; for 24h; Heating;

DOI:10.3891/acta.chem.scand.50-0938

Reference yield: 21.0%

N,N'-diacetyl-trans-1,2-diaminocyclohexane (54009-70-0,70924-77-5,70924-78-6) → N-((1S,2S)-2-Thioacetylamino-cyclohexyl)-acetamide + N-((1S,2S)-2-Thioacetylamino-cyclohexyl)-thioacetamide

Guidance literature:

With 2,4-bis<4-(methylthio)phenyl>-1,3,2,4-dithiadiphosphetane 2,4-disulfide; In toluene; for 24h; Heating;

DOI:10.3891/acta.chem.scand.50-0938

upstream raw materials:

trans-1,2-Diaminocyclohexane

acetic anhydride