2-{(E)-[(2-Nitrophenyl)methylidene]amino}benzoic acid

Base Information

Chemical Name:2-{(E)-[(2-Nitrophenyl)methylidene]amino}benzoic acid
CAS No.:63002-97-1
Molecular Formula:C₁₄H₁₀N₂O₄
Molecular Weight:270.244
Hs Code.:
NSC Number:405395
DSSTox Substance ID:DTXSID70323995

Synonyms:63002-97-1;NSC405395;DTXSID70323995;NSC-405395;2-{(E)-[(2-Nitrophenyl)methylidene]amino}benzoic acid

Suppliers and Price of 2-{(E)-[(2-Nitrophenyl)methylidene]amino}benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-{(E)-[(2-Nitrophenyl)methylidene]amino}benzoic acid

Chemical Property:

Vapor Pressure:1.01E-11mmHg at 25°C
Boiling Point:522°C at 760 mmHg
Flash Point:269.5°C
Density:1.31g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:270.06405680
Heavy Atom Count:20
Complexity:391

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C=NC2=CC=CC=C2C(=O)O)[N+](=O)[O-]

Technology Process of 2-{(E)-[(2-Nitrophenyl)methylidene]amino}benzoic acid

There total 1 articles about 2-{(E)-[(2-Nitrophenyl)methylidene]amino}benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 552-89-6
2-nitro-benzaldehyde

: 63002-97-1
N-(2-nitro-benzyliden)-anthranilic acid

Guidance literature:: With ethanol;

Reference yield: 80.0%

: 63002-97-1
N-(2-nitrobenzylidene)-2-carboxyaniline

: thorium(IV) chloride * xH₂O

: Th(Cl)2{C₆H₄(COO)NCHC₆H₄(NO₂)}2

Guidance literature:: In ethanol; stirring of Th-salt and ligand in warm ethanol under dry nitrogen for 30 min; filtn., washing (ethanol, then with diethyl ether), drying invacuo for 6 h at 120°C, elem. anal.;
DOI:10.1016/S0020-1693(00)84854-9

Reference yield: 68.0%

: thorium(IV) nitrate hydrate

: 63002-97-1
N-(2-nitrobenzylidene)-2-carboxyaniline

: Th(NO₃)2{C₆H₄(COO)NCHC₆H₄(NO₂)}2

Guidance literature:: In ethanol; stirring of Th-salt and ligand in warm ethanol under dry nitrogen for 30 min; filtn., washing (ethanol, then with diethyl ether), drying invacuo for 6 h at 120°C, elem. anal.;
DOI:10.1016/S0020-1693(00)84854-9