(2-dimethylaminomethylbenzyl)methylphenyltin bromide

Base Information

• Chemical Name: (2-dimethylaminomethylbenzyl)methylphenyltin bromide
• CAS No.: 60528-56-5
• Molecular Formula: C₁₇H₂₂BrNSn
• Molecular Weight: 438.982
• Mol file: 60528-56-5.mol

Synonyms:

Chemical Property of (2-dimethylaminomethylbenzyl)methylphenyltin bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (2-dimethylaminomethylbenzyl)methylphenyltin bromide

There total 1 articles about (2-dimethylaminomethylbenzyl)methylphenyltin bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(o-{(dimethylamino)methyl}phenyl)methyllithium (60528-54-3) + phenyl methyl tin dibromide (21247-36-9) → (2-dimethylaminomethylbenzyl)methylphenyltin bromide (60528-56-5)

Guidance literature:

In diethyl ether; byproducts: LiBr; under N2 organo-lithium compd. in ether added slowly to a soln. of SnMePhBr2 in ether, mixt. stirred for 1 h; ether removed in vac., residue dissolved in benzene, LiBr filtered off,filtrate concd., residue dissolved in benzene, pentane added to it, crystals filtered off, washed with pentane, dried in vac.; elem. anal.;

DOI:10.1039/DT9800001352

upstream raw materials:

(o-{(dimethylamino)methyl}phenyl)methyllithium

phenyl methyl tin dibromide