tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:130259-26-6
Molecular Formula:C₅₃H₇₇N₅O₁₄Si
Molecular Weight:1036.3
Hs Code.:

tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 4 articles about tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyldimethylsilyl 2-azido-4-O-<2-azido-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 130259-26-6
tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With hydrogen sulfide; In pyridine; water; for 24h;
DOI:10.1016/0008-6215(90)84080-E

Reference yield:

: 120312-09-6
tert-Butyldimethylsilyl-2-azido-3,6-di-O-benzyl-2-desoxy-β-D-glucopyranosid

: 130259-26-6
tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / BF₃*Et₂O / CH₂Cl₂ / 14 h

3: H₂S / pyridine; H₂O / 24 h

With boron trifluoride diethyl etherate; hydrogen sulfide; In pyridine; dichloromethane; water;
DOI:10.1016/0008-6215(90)84080-E

Reference yield:

: tert-butyldimethylsilyl 2-azido-4-O-<2-azido-2-deoxy-4,6-O-isopropylidene-3-O-<(1R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 130259-26-6
tert-butyldimethylsilyl 2-amino-4-O-<2-amino-2-deoxy-4,6-O-isopropylidene-3-O-<(2R)-propanoyl-(L-alanyl-D-isoglutamine benzyl ester)-2-yl>-β-D-glucopyranosyl>-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

2: H₂S / pyridine; H₂O / 24 h

With hydrogen sulfide; In pyridine; water;
DOI:10.1016/0008-6215(90)84080-E