Boc-PheΨGly-Sta-Leu-NHCH2Ph

Base Information

Chemical Name:Boc-PheΨGly-Sta-Leu-NHCH2Ph
CAS No.:118405-13-3
Molecular Formula:C₃₈H₅₈N₄O₆
Molecular Weight:666.902
Hs Code.:

Synonyms:

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Chemical Property of Boc-PheΨGly-Sta-Leu-NHCH2Ph

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Technology Process of Boc-PheΨGly-Sta-Leu-NHCH2Ph

There total 3 articles about Boc-PheΨGly-Sta-Leu-NHCH2Ph which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82042-48-6
(S)-5-<(tert-Butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoic acid

: 118405-13-3,124338-92-7
Boc-PheΨGly-Sta-Leu-NHCH2Ph

Guidance literature:: Multi-step reaction with 2 steps

1: 0.45 g / H₂ / 10percent Pd/C / propan-2-ol / 20 °C / 2637.5 Torr

2: HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp.

With hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm00164a058

Reference yield:

: 82001-64-7
(E)-(S)-<1-(phenylmethyl)-5-(trimethylsilyl)-3-hexen-5-ynyl>carbamic acid 1,1-dimethylethyl ester

: 118405-13-3,124338-92-7
Boc-PheΨGly-Sta-Leu-NHCH2Ph

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) (cyclohexyl)2BH, 2.) 2 N NaOH, 30percent H₂O₂ / 1.) THF, 0 deg C, 1 h, 2.) MeOH, room temp., 1 h

2: 0.45 g / H₂ / 10percent Pd/C / propan-2-ol / 20 °C / 2637.5 Torr

3: HOBT/DCC, Et₃N / dimethylformamide / 1.) 0 deg C, 0.5 h, 2.) room temp.

With sodium hydroxide; bis(cyclohexanyl)borane; hydrogen; dihydrogen peroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm00164a058

Reference yield:

: 118387-85-2
Boc-PheΨGly

: 118405-13-3,124338-92-7
Boc-PheΨGly-Sta-Leu-NHCH2Ph

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1.) 0 deg C, 0.5 h, 2.) room temp.;
DOI:10.1021/jm00164a058