6a-Phenyl-6a-(1,3,5,7-tetramethyl-2,6-dioxo-1,3,5,7-tetraaza-4λ⁵-phospha-spiro[3.3]hept-4-yl)-1,6-dioxa-3a-aza-6aλ⁵-phospha-pentalene-2,5-dione

Base Information

• Chemical Name: 6a-Phenyl-6a-(1,3,5,7-tetramethyl-2,6-dioxo-1,3,5,7-tetraaza-4λ⁵-phospha-spiro[3.3]hept-4-yl)-1,6-dioxa-3a-aza-6aλ⁵-phospha-pentalene-2,5-dione
• CAS No.: 129868-33-3
• Molecular Formula: C₁₆H₂₁N₅O₆P₂
• Molecular Weight: 441.32

Synonyms:

Chemical Property of 6a-Phenyl-6a-(1,3,5,7-tetramethyl-2,6-dioxo-1,3,5,7-tetraaza-4λ⁵-phospha-spiro[3.3]hept-4-yl)-1,6-dioxa-3a-aza-6aλ⁵-phospha-pentalene-2,5-dione

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 6a-Phenyl-6a-(1,3,5,7-tetramethyl-2,6-dioxo-1,3,5,7-tetraaza-4λ⁵-phospha-spiro[3.3]hept-4-yl)-1,6-dioxa-3a-aza-6aλ⁵-phospha-pentalene-2,5-dione

There total 1 articles about 6a-Phenyl-6a-(1,3,5,7-tetramethyl-2,6-dioxo-1,3,5,7-tetraaza-4λ⁵-phospha-spiro[3.3]hept-4-yl)-1,6-dioxa-3a-aza-6aλ⁵-phospha-pentalene-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

8-Phenyl-8λ5-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole-2,6-dione (81741-70-0) + 4-Chloro-1,3,5,7-tetramethyl-1,3,5,7-tetraaza-4λ5-phosphabicyclo<3.3>heptan-2,6-dion (77507-70-1) → 6a-Phenyl-6a-(1,3,5,7-tetramethyl-2,6-dioxo-1,3,5,7-tetraaza-4λ5-phospha-spiro[3.3]hept-4-yl)-1,6-dioxa-3a-aza-6aλ5-phospha-pentalene-2,5-dione (129868-33-3)

Guidance literature:

With triethylamine; In tetrahydrofuran;

DOI:10.1016/S0040-4020(01)81521-0

upstream raw materials:

8-Phenyl-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole-2,6-dione

4-Chloro-1,3,5,7-tetramethyl-1,3,5,7-tetraaza-4λ⁵-phosphabicyclo<3.3>heptan-2,6-dion

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